Dear Takaai 

You have to specify link records yourself to be used by REFMAC.

Use JLIGAND for link records see
http://www.ysbl.york.ac.uk/mxstat/JLigand/tutorial_link.html

Cheers
Stefan

-----Ursprüngliche Nachricht-----
Von: Mailing list for users of COOT Crystallographic Software
[mailto:[email protected]] Im Auftrag von Takaaki Fukami
Gesendet: Mittwoch, 18. Januar 2012 08:00
An: [email protected]
Betreff: Re: N-terminal ACE restraints

Dear Paul,

Coot handles the ACE group properly, though it won't write any LINK record
to a pdb file to refine it by refmac. Therefore, the ACE group moved away in
the refined structure.

Could you make Coot to write out the LINK records at leaset present in an
input pdb file?

Regards,

Takaaki


-----Original Message-----
From: Paul Emsley [mailto:[email protected]]
Sent: Tuesday, January 17, 2012 9:47 PM
Subject: Re: N-terminal ACE restraints

On 17/01/12 12:01, Takaaki Fukami wrote:
> Dear Coot experts,
>
> I have a protein with an N-acetyl group at its N-terminal, and want to 
> refine it with coot & refmac5.
> Refmac recognize the LINK and applied restraints in
$CLIB/list/mon_lib_list.cif.
>
> In Coot, when I "refine zone" from B0 to B1, the ACE group moved away 
> from the next PHE. They won't connect each other.

Try sphere refine, that has more sophisticated linking rules.

>
> I extracted the data_link_ACE_C-N section from the mon_lib_list.cif 
> file and import it into Coot, but it didn't work.
>
> How do I include the link restraints into Coot?
>

It should Just Work. If it doesn't then I need to fix it. I've added this to
my list.

LINKRs for refinement are scheduled for 0.8.

Regards,

Paul.

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