http://pubs.acs.org/doi/abs/10.1021/acs.energyfuels.6b00527

Kinetics of carbon dioxide removal by n-propyl- and
n-butyl-monoethanolamine in aqueous solutions

Ravindra B. Kanawade, Prakash D. Vaidya, Krishnan Subramanian, Vijay V
Kulkarni and Eugeny Y. Kenig

Energy & Fuels

Publication Date (Web): May 18, 2016

DOI: 10.1021/acs.energyfuels.6b00527

Secondary alkanolamines associated with an alkyl group are potentially
attractive post-combustion CO2-capturing solvents. Their reactivity with
CO2 is influenced by the nature of the alkyl group that substitutes the
hydrogen atom of the amino functional group. In the present work, we
measured the rates of CO2 absorption into aqueous solutions of
n-propylmonoethanolamine (PMEA) and n-butylmonoethanolamine (BMEA) in a
stirred cell reactor under fast pseudo-first order conditions. The
concentrations of PMEA and BMEA in the water solutions were changed in the
2-3 kmol m-3 range. It was discovered that, unlike the usual amines, PMEA
and BMEA followed overall third-order kinetics. We evaluated the reaction
rate constants at different temperatures, viz. 303, 308 and 313 K and
discovered that PMEA reacts with CO2 faster than BMEA. Furthermore, we gave
an interpretation of the kinetic data using the zwitterion and termolecular
mechanisms. Finally, a comparison of the efficacy of the investigated
solvents with N-methylmonoethanolamine (MMEA) and N-ethylmonoethanolamine
(EMEA) was accomplished. It was found that reactivity of amines diminished
in the order EMEA>MMEA>PMEA>BMEA

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