Hi All, 

A new paper of potential interest: 

Mie scattering from optically levitated mixed sulfuric acid–silica 
core–shell aerosols: observation of core–shell morphology for atmospheric 
science

https://pubs.rsc.org/en/content/articlelanding/2022/CP/D1CP04068E

*Potential Stratospheric Aerosol Injection (SAI) implications*

There's been various papers (my own included) that have suggested that 
materials other than sulphate would be optimal for light scattering and 
weight lifting considerations for SAI, e.g. alumina, titania, diamond 
etc... This paper suggests that the collision and coating of sulphuric acid 
on solid aerosol particles would cause the benefits of the solid particle 
scattering to diminish rapidly, with the scattering properties being driven 
by sulphuric acid coating.  So you might as well use sulphuric acid / 
sulphate aerosols in the first place. 

Note - useful further work would repeat the experiments at stratospheric 
temperatures (this lab work was conducted at room temperature) and the 
coagulation dynamics needs to be explored to see how long it would take for 
a sufficient sulphuric acid coating to be generated upon the injected 
particles. 


Abstract

Sulfuric acid is shown to form a core–shell particle on a micron-sized, 
optically-trapped spherical silica bead. The refractive indices of the 
silica and sulfuric acid, along with the shell thickness and bead radius 
were determined by reproducing Mie scattered optical white light as a 
function of wavelength in Mie spectroscopy. Micron-sized silica aerosols 
(silica beads were used as a proxy for atmospheric silica minerals) were 
levitated in a mist of sulfuric acid particles; continuous collection of 
Mie spectra throughout the collision of sulfuric acid aerosols with the 
optically trapped silica aerosol demonstrated that the resulting aerosol 
particle had a core–shell morphology. Contrastingly, the collision of 
aqueous sulfuric acid aerosols with optically trapped polystyrene aerosol 
resulted in a partially coated system. The light scattering from the 
optically levitated aerosols was successfully modelled to determine the 
diameter of the core aerosol (±0.003 μm), the shell thickness (±0.0003 μm) 
and the refractive index (±0.007). The experiment demonstrated that the 
presence of a thin film rapidly changed the light scattering of the 
original aerosol. When a 1.964 μm diameter silica aerosol was covered with 
a film of sulfuric acid 0.287 μm thick, the wavelength dependent Mie peak 
positions resembled sulfuric acid. Thus mineral aerosol advected into the 
stratosphere would likely be coated with sulfuric acid, with a core–shell 
morphology, and its light scattering properties would be effectively 
indistinguishable from a homogenous sulfuric acid aerosol if the film 
thickness was greater than a few 100 s of nm for UV-visible wavelengths.


4 Conclusions

The study presented here demonstrates that sulfuric acid successfully forms 
a core–shell geometry aerosol upon collision with silica. Through 
application of optical trapping techniques alongside Mie spectroscopy, it 
was observed that when a sulfuric acid aerosol collides with a silica 
aerosol, the system would begin to resemble a sulfuric acid aerosol of 
similar diameter to the combined aerosol. Secondly, the study 
experimentally demonstrates that mineral aerosol emitted to the 
stratosphere will soon adopt the light scattering patterns associated with 
a pure sulfuric acid aerosol. The implication of the study to stratospheric 
science is that hydrophilic stratospheric mineral aerosol will rapidly 
resemble the optical properties of sulfuric acid through natural collision 
processes and the formation of core–shell morphology.


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