Hi,

the paper on Mie scattering is very interesting and it is an important addition 
to the small number of experimental studies for alternate materials for 
stratospheric aerosol injection.

It is worth noting that the sulfuric acid coatings on silica are however very 
large in the study. The thinnest coating, after one collision, was achieved via 
collision with a 4 um^3 sulfuric acid particle, much larger than found in the 
stratosphere with average sulfuric acid aerosol radii of 0.08 um (~10/cm3). In 
the paper, after this first collision,  already ~50% of the volume consist of 
sulfuric acid. Given, that the total stratospheric load of sulfuric acid 
aerosol is around 0.46 Mt H2SO4 even in a moderate scenario of 1MT Al2O3 
injection/year there is not enough sulfuric acid to form such a thick coating. 
In fact, a fully coupled model we are currently running with 5MT Al2O3 
injections/year shows coating thicknesses of <1 - 25 nm on alumina in the 
stratosphere depending on the radius of the emitted particles (80-320nm), with 
the majority of particles having thicknesses below 10nm. This is for particles 
at high latitudes (far from the injection latitude) which have the largest 
coating thicknesses.

My point mainly is that, yes, if a large fraction or majority of the volume 
consists of sulfuric acid, the scattering properties are close to those of 
sulfuric acid. However, for scenarios that would be relevant for potential 
stratospheric aerosol injection with alternate materials that is not the case.

Lastly, from my perspective, the main reason for exploring alternate materials 
is not tied to scattering efficiency, but rather to potentially reducing risk 
from the stratospheric heating and perhaps ozone destruction.

It is definitely great to see more laboratory studies of alternate materials 
for SAI!

All the best,

Frank


___________________________________________________________________________________________
Frank N. Keutsch
Stonington Professor of Engineering and Atmospheric Science

Harvard John A. Paulson School of Engineering and Applied Sciences
Department of Chemistry and Chemical Biology
Department of Earth and Planetary Sciences
Harvard University
12 Oxford Street
Cambridge, MA 02138
USA

E-mail:
[email protected]<mailto:[email protected]>

Tel:+1-617-495-1878
___________________________________________________________________________________________


From: <[email protected]> on behalf of Francis Pope 
<[email protected]>
Reply-To: "[email protected]" <[email protected]>
Date: Tuesday, March 1, 2022 at 11:59 AM
To: geoengineering <[email protected]>
Subject: [geo] Mie scattering from optically levitated mixed sulfuric 
acid–silica core shell aerosols

Hi All,

A new paper of potential interest:

Mie scattering from optically levitated mixed sulfuric acid–silica core–shell 
aerosols: observation of core–shell morphology for atmospheric science

https://pubs.rsc.org/en/content/articlelanding/2022/CP/D1CP04068E<https://urldefense.proofpoint.com/v2/url?u=https-3A__pubs.rsc.org_en_content_articlelanding_2022_CP_D1CP04068E&d=DwMFaQ&c=WO-RGvefibhHBZq3fL85hQ&r=SxgtIVByLvhD8QiO8rgwrvm9f9GML9Drha7439cd21U&m=ouQdAL9_Hinqa8MYv8CnkUl8Ufmbp0NR7G5txWzSQzjsk5mw9xW77OHfx4iSQ5gr&s=4KRdQPlWpnlvoJrgigjGqu4upxd7o-Mn8Otmo2CHKU8&e=>


Potential Stratospheric Aerosol Injection (SAI) implications

There's been various papers (my own included) that have suggested that 
materials other than sulphate would be optimal for light scattering and weight 
lifting considerations for SAI, e.g. alumina, titania, diamond etc... This 
paper suggests that the collision and coating of sulphuric acid on solid 
aerosol particles would cause the benefits of the solid particle scattering to 
diminish rapidly, with the scattering properties being driven by sulphuric acid 
coating.  So you might as well use sulphuric acid / sulphate aerosols in the 
first place.

Note - useful further work would repeat the experiments at stratospheric 
temperatures (this lab work was conducted at room temperature) and the 
coagulation dynamics needs to be explored to see how long it would take for a 
sufficient sulphuric acid coating to be generated upon the injected particles.


Abstract

Sulfuric acid is shown to form a core–shell particle on a micron-sized, 
optically-trapped spherical silica bead. The refractive indices of the silica 
and sulfuric acid, along with the shell thickness and bead radius were 
determined by reproducing Mie scattered optical white light as a function of 
wavelength in Mie spectroscopy. Micron-sized silica aerosols (silica beads were 
used as a proxy for atmospheric silica minerals) were levitated in a mist of 
sulfuric acid particles; continuous collection of Mie spectra throughout the 
collision of sulfuric acid aerosols with the optically trapped silica aerosol 
demonstrated that the resulting aerosol particle had a core–shell morphology. 
Contrastingly, the collision of aqueous sulfuric acid aerosols with optically 
trapped polystyrene aerosol resulted in a partially coated system. The light 
scattering from the optically levitated aerosols was successfully modelled to 
determine the diameter of the core aerosol (±0.003 μm), the shell thickness 
(±0.0003 μm) and the refractive index (±0.007). The experiment demonstrated 
that the presence of a thin film rapidly changed the light scattering of the 
original aerosol. When a 1.964 μm diameter silica aerosol was covered with a 
film of sulfuric acid 0.287 μm thick, the wavelength dependent Mie peak 
positions resembled sulfuric acid. Thus mineral aerosol advected into the 
stratosphere would likely be coated with sulfuric acid, with a core–shell 
morphology, and its light scattering properties would be effectively 
indistinguishable from a homogenous sulfuric acid aerosol if the film thickness 
was greater than a few 100 s of nm for UV-visible wavelengths.



4 Conclusions

The study presented here demonstrates that sulfuric acid successfully forms a 
core–shell geometry aerosol upon collision with silica. Through application of 
optical trapping techniques alongside Mie spectroscopy, it was observed that 
when a sulfuric acid aerosol collides with a silica aerosol, the system would 
begin to resemble a sulfuric acid aerosol of similar diameter to the combined 
aerosol. Secondly, the study experimentally demonstrates that mineral aerosol 
emitted to the stratosphere will soon adopt the light scattering patterns 
associated with a pure sulfuric acid aerosol. The implication of the study to 
stratospheric science is that hydrophilic stratospheric mineral aerosol will 
rapidly resemble the optical properties of sulfuric acid through natural 
collision processes and the formation of core–shell morphology.


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