Dear all,
I had a strange peak at lower angle (003, ~22 2theta) collected from LiCoO2 (R
-3 m).
It's a single phase powder diffraction and only one peak as in ICSD database
2013.
The peak getting more unreasonable as I heated, (but it still single phase)
Please take a look the profiles: LiCoO2-003.JPG
LiCoO2-003.JPG
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I tried to use S/L in GSAS-II but the value is not reasonable S/L >
0.177570E-01 (L=173mm).
Thanks for the attention.
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