Hi Armel,
I am sure you will not be satisfied by this answer, but my solution to
this problem is : USE transmission geometry. We have been doing it for
years getting nice results for kaolinites, micas, vermiculites and
smectites, not to
speak of some organic plates. No need to add -osils (what's that, BTW). 
Lubo

P.S. I am not adding the type of diffractometer, but if you wish I can
scan a sample for you .... 

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