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Dear Rietvelders
I am trying to refine (fullprof) x-ray (Cu Ka)
pattern of spinel CuTi2(S,Se)4 which was measured in flat specimen sample
holder in D8 Th:Th without monochromator (10-158 2Th). the experiment
details were step each 0.02 2Th with 10 sec per step. the background was
subtructed in EVA.
the problem that i am facing
is that the R_Bragg is 3.71 but the
global chi2 is 7.5 only if i am excluded the region to 10 - 80 2Th. what can be
the reason for that?
Thank's in advance for your ideas
Eli
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- Re: global chi2 eli
- Re: global chi2 Miguel Hesiquio Gardu?o
- Conversion software available? Dr. K. Selvaraj
- Re: Conversion software available? Magnus H. Sorby
- Re: Conversion software available? Brian H. Toby
- RE: global chi2 TRILLON Gilbert
