Dear Mirela, if you are working with quartz capillaries, i would use Pt for the filament. The plastic parts on the connectors can be removed. I actually did this already in the basic design. Let me know if you can reach the necessary temperature!
Best Miguel El mié, 1 feb. 2023 8:18, miguel gregorkiewitz <gregorm...@gmail.com> escribió: > Dear Mirela, > > A couple of minutes ago I sent you a zip file containg the documents of > our manipulator to seal capillaries etc. > > Let me know if you have any.problems! > > Best > > Miguel > > El mié, 1 feb. 2023 0:22, mirela dragomir <dragomir.mir...@yahoo.com> > escribió: > >> Dear Miguel, >> >> I'm also intrigued by your setup and would like to learn more. Currently, >> we are sealing our quartz capillaries outside of the glove box. >> >> Thank you and best regards, >> >> Mirela >> >> ------------------------ >> >> Asst. Prof. Mirela Dragomir >> >> Electronic Ceramics Department, K5 >> >> http://www-k5.ijs.si/ >> >> Jožef Stefan Institute >> >> Jamova cesta 39, 1000 Ljubljana, Slovenia >> >> Associate Editor, Acta Chimica Slovenica >> >> https://acta.chem-soc.si/ >> >> E-mail: mirela.drago...@ijs.si >> >> Web: http://eccl.ijs.si/ >> >> Phone: +386 1 477 3512 >> >> >> >> On Monday, January 30, 2023 at 01:10:41 PM GMT+1, miguel gregorkiewitz < >> gregorm...@gmail.com> wrote: >> >> >> I constructed an electrical heater which is used with a tunable power >> supply and a microscope if possible. Let me know if you like to have >> details of the design! >> >> Miguel >> >> >> El lun, 30 ene. 2023 12:01, francois Goutenoire < >> francois.gouteno...@univ-lemans.fr> escribió: >> >> Dear Rietveld users, >> >> We are currently working with some very hygroscopic compounds in >> capillaries. >> >> These capillaries are fill in a glove box (N2). >> >> How can we sealed these capillaries (borosilicate) in the glove box ? >> >> Best wishes, François >> >> -- >> ********************************************************************************************* >> Pr. Francois GOUTENOIRE >> e-mail: francois.gouteno...@univ-lemans.fr >> Tel: 02.43.83.33.54 >> FAX: 02.43.83.35.06 >> Institut des Molécules et des Matériaux du Mans >> IMMM - UMR CNRS 6283 >> Elaboration et Caracterisation des Composés Cristalisés (E3C) >> Université du Maine - Avenue Olivier Messiaen >> F-72085 Le Mans Cedex 9 >> FRANCE >> ********************************************************************************************* >> Formation Rietveld >> CNRShttps://cnrsformation.cnrs.fr/diffraction-des-rayons-x-sur-materiaux-polycristallins?axe=135 >> Formation EDX CNRShttps://cnrsformation.cnrs.fr/fluorescence-x-edx?axe=135 >> Formation SAXS et Réflectivités pour couches minces et matériaux >> nanostructurés.https://cnrsformation.cnrs.fr/caracterisation-des-materiaux-nanostructures-par-diffusion-des-rayons-x?axe=135 >> Bibliographiehttps://scholar.google.fr/citations?hl=fr&user=qC-lmN4AAAAJ&view_op=list_works&authuser=1&sortby=titlehttps://orcid.org/0000-0001-5339-3002 >> >> ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ >> Please do NOT attach files to the whole list <alan.he...@neutronoptics.com >> > >> Send commands to <lists...@ill.fr> eg: HELP as the subject with no body >> text >> The Rietveld_L list archive is on >> http://www.mail-archive.com/rietveld_l@ill.fr/ >> ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ >> >> ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ >> Please do NOT attach files to the whole list < >> alan.he...@neutronoptics.com> >> Send commands to <lists...@ill.fr> eg: HELP as the subject with no body >> text >> The Rietveld_L list archive is on >> http://www.mail-archive.com/rietveld_l@ill.fr/ >> ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ >> >>
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