Re: EXTERNAL: RE: [Vo]:MIT Course Day 5 -- NiH Systems

2014-02-08 Thread Bob Higgins
Hi Eric,

I have made progress and have constructed a new reactor optimized to allow
low energy photons to escape.  These would be unmistakable signatures of
LENR without having to be so optimized to show excess heat to the extent it
proves a nuclear source.  I have seen transient heat bursts and I want to
correlate these with emitted photons.

Unfortunately, I am on a temporary hold to get myself and my little lab
moved across the US to NM.

Bob


On Fri, Feb 7, 2014 at 10:49 PM, Eric Walker eric.wal...@gmail.com wrote:

 On Fri, Feb 7, 2014 at 7:43 AM, Bob Higgins rj.bob.higg...@gmail.comwrote:

 Rossi has stated that he starts with 10 micron sized particles (since
 identified as a nickel powder produced from the carbonyl process), adds a
 catalyst (widely believed to be a nanopowder of some kind), and processes
 the mix in a way that leads to amplified tubercles on the surface.


 Thanks for the helpful clarification.  I didn't realize that.  The main
 reference I have found is Hank Mills's PESN article [1].  I'm curious where
 Mills got this information.

 It sounds like you have made a lot of progress on getting an NiH reactor
 set up.  Have you seen anything interesting?

 Eric


 [1]
 http://pesn.com/2012/01/02/9601998_Defkalion_Claims_No_Problem_with_Revealing_Cold_Fusion_Catalyst/




RE: EXTERNAL: RE: [Vo]:MIT Course Day 5 -- NiH Systems

2014-02-07 Thread Roarty, Francis X
IMHO grain size and geometry of these other alloys as powders will have a 
major effect on their LENR activity.
Fran

From: Jones Beene [mailto:jone...@pacbell.net]
Sent: Thursday, February 06, 2014 5:16 PM
To: vortex-l@eskimo.com
Subject: EXTERNAL: RE: [Vo]:MIT Course Day 5 -- NiH Systems

From: Jed Rothwell

Superior for what? Conducting protons? Surely not for loading hydrogen. I have 
never heard that.

Surely you read Ahern's Arata replication for EPRI ?

He achieved better loading than the standard of 1:1 with nickel-palladium alloy 
(at low Pd ratio in the alloy).

Many alloys which are tailored for hydrogen storage are in fact better than 
palladium for that single property (which is the atomic ratio of lattice atoms 
to hydrogen atoms)

This does not meant they will be more active for LENR - only that they will 
absorb more atoms of hydrogen per atom of lattice. That is what they are 
designed for.

In fact, the alloys which store the most hydrogen are most often NOT anomalous 
as to energy release, when further stimulated. Unfortunately, the two fields 
have not been systematically investigated for determining the best of both 
worlds.

Jones


RE: EXTERNAL: RE: [Vo]:MIT Course Day 5 -- NiH Systems

2014-02-07 Thread Roarty, Francis X
Bob,
Much discussion regarding micro “tubule” geometry of Rossi  powders 
leads many of us to consider the hair like protrusions as forming nano geometry 
between the grains as they pack to form a bulk powder.
Fran

_
From: Jones Beene [mailto:jone...@pacbell.net]
Sent: Thursday, February 06, 2014 5:50 PM
To: vortex-l@eskimo.com
Subject: EXTERNAL: RE: [Vo]:MIT Course Day 5 -- NiH Systems


-Original Message-
From: Bob Cook

   Also I suspect that the nano Ni that is produced is pretty pure. That 
 may be why Rossi uses it …

Not sure that I follow this. Although the Rossi patent mentions nanometric 
and specifically a favored isotope - Rossi himself has identified his nickel 
supplier, and says the geometry of his powder is micron not nano (at least at 
that point in time). Metals (as opposed to ceramics) can seldom be reduced 
below 10 microns by normal Industrial methods such as ball milling - due to 
surface electric properties aka: “agglomeration.”

That is one reason why “nano” is so special and not fully appreciated wrt 
metals. It simply cannot happen in normal metal processing (except with mixed 
ceramics like the oxides of nickel). You might do well to talk to the Ni-O 
“nano” suppliers, like Quantum sphere:

http://www.qsinano.com/products_nanomaterials.html

They will set you straight on the lack of anything truly “nano” as a metal. It 
must have a surface oxide.

   … and may be the reason other researchers do not have very good luck at 
 getting a good reaction.

No doubt that Rossi, if we can believe his results, has found something that no 
one else has yet been able to duplicate. It may be serendipitous, but it is not 
likely to be “nanometric nickel” per se.

Jones



RE: EXTERNAL: RE: [Vo]:MIT Course Day 5 -- NiH Systems

2014-02-07 Thread Jones Beene

From: Roarty, Francis X 
Bob,
Much discussion regarding micro “tubule” geometry of
Rossi powders leads many of us to consider the hair like protrusions as
forming nano geometry between the grains as they pack to form a bulk powder.
Fran

The tubes could be hollow as well as in Enculescu’s  image below. 

Does anyone  have the citation for Rossi’s nickel lattice having “tubules”?
Cannot find it. But check this out.

http://www.science24.com/paper/11457

This is a marvelous image of what can be done, in principal, with nickel
nanotubes via electroless deposition. It would not surprise me if Rossi’s
supplier of nickel has used a similar technique.

This particular paper is Romanian/German and has no connection to LENR that
I am aware of. I wonder if Peter Gluck is aware of it?

Perhaps a gram or two of this actual material should be tried in LENR, due
to the possibility of entrapment of hydrogen in the tubes in one dimension,
as we have discussed.

As a caveat, this electroless nickel deposition technique apparently
involves high phosphorous content, which could be a poison (who knows?)
_
From: Jones Beene  
 
-Original Message-
From: Bob Cook 
 
*   Also I suspect that the nano Ni that is produced is pretty pure.
That may be why Rossi uses it …
 
Not sure that I follow this. Although the Rossi patent
mentions nanometric and specifically a favored isotope - Rossi himself has
identified his nickel supplier, and says the geometry of his powder is
micron not nano (at least at that point in time). Metals (as opposed to
ceramics) can seldom be reduced below 10 microns by normal Industrial
methods such as ball milling - due to surface electric properties aka:
“agglomeration.” 
 
That is one reason why “nano” is so special and not fully
appreciated wrt metals. It simply cannot happen in normal metal processing
(except with mixed ceramics like the oxides of nickel). You might do well to
talk to the Ni-O “nano” suppliers, like Quantum sphere:
 
http://www.qsinano.com/products_nanomaterials.html
 
They will set you straight on the lack of anything truly
“nano” as a metal. It must have a surface oxide.
 
*   … and may be the reason other researchers do not have very good luck
at getting a good reaction. 
 
No doubt that Rossi, if we can believe his results, has
found something that no one else has yet been able to duplicate. It may be
serendipitous, but it is not likely to be “nanometric nickel” per se.
 
Jones
 
attachment: winmail.dat

Re: EXTERNAL: RE: [Vo]:MIT Course Day 5 -- NiH Systems

2014-02-07 Thread ChemE Stewart
morphing through some kind of process of entropy

I think you are right, Vacuum = Entropy = Uncertainty!


On Fri, Feb 7, 2014 at 10:00 AM, Eric Walker eric.wal...@gmail.com wrote:

 On Fri, Feb 7, 2014 at 6:53 AM, Jones Beene jone...@pacbell.net wrote:

 Does anyone  have the citation for Rossi's nickel lattice having tubules?
 Cannot find it. But check this out.


 Yes, please.  If anyone has a reference to Rossi using nickel with
 tubules, nanotubules, nanohairs, etc., please provide it.  My
 understanding is that he uses micron-sized nickel powder, treated in some
 way, and rather than something nano-.  There are carbon nanotubes, of
 course, and Rossi, as far as anyone knows, does not use them.

 It's remarkably difficult to pin the precise details down and keep them
 pinned down.  They keep on moving around and morphing through some kind of
 process of entropy.

 Eric




RE: EXTERNAL: RE: [Vo]:MIT Course Day 5 -- NiH Systems

2014-02-07 Thread Jones Beene
As Eric realizes, this is a critical issue for anyone wanting to replicated 
Rossi.

 

In fact, the material shown in the previous image, could indeed be called 
“micron sized” and one would not be dishonest. However the importance of hollow 
nickel tube could be the sine qua non of the Rossi scheme.

 

Rossi has a history in his revelations, at least back when he was in full 
fund-raising mode, of first providing a bit too much information 
(inadvertently) and then backtracking later to try to minimize the damage.

 

Thus, we often see conflicting statements which can be rationalized if one 
understands the history of “Rossi-speak”. 

 

This “tubule” mystery could be an exemplary example of what I am talking about. 
But did he actually ever say it?

 

From: Eric Walker 

 

Does anyone  have the citation for Rossi’s nickel lattice having “tubules”?
Cannot find it. But check this out.

 

Yes, please.  If anyone has a reference to Rossi using nickel with tubules, 
nanotubules, nanohairs, etc., please provide it.  My understanding is that 
he uses micron-sized nickel powder, treated in some way, and rather than 
something nano-.  There are carbon nanotubes, of course, and Rossi, as far as 
anyone knows, does not use them.

 

It's remarkably difficult to pin the precise details down and keep them pinned 
down.  They keep on moving around and morphing through some kind of process of 
entropy.

 

Eric

 



Re: EXTERNAL: RE: [Vo]:MIT Course Day 5 -- NiH Systems

2014-02-07 Thread Bob Higgins
Rossi has stated that he starts with 10 micron sized particles (since
identified as a nickel powder produced from the carbonyl process), adds a
catalyst (widely believed to be a nanopowder of some kind), and processes
the mix in a way that leads to amplified tubercles on the surface.

A search of tubules will not find the reference, he used tubercles.

I have replicated the growth of tubercles by doing just what Rossi
described.  Begin with micron scale nickel powder (from the carbonyl
precipitate process), add a nanopowder, mix, and heat in an oven with
cycling H2, Ar, O2 process gas.  The result is a porous structure of
tubercles with nanowires growing from the surface.  I suspect that both
the nanowires and the tubercle structure are indicators that I am using
similar processing of the powder mix as Rossi, but are not themselves the
LENR NAE.  The observation is that when processed in that manner, there are
plenty of NAE somewhere.  It is easy to believe that this structure (from
the SEM pictures) will be rife with nanocracks as Dr. Storms suggests for
the NAE.  In fact, the NAE are likely to be features you cannot see under
the SEM rather than the features you can see.

Bob Higgins


On Fri, Feb 7, 2014 at 10:12 AM, Jones Beene jone...@pacbell.net wrote:

  As Eric realizes, this is a critical issue for anyone wanting to
 replicated Rossi.



 In fact, the material shown in the previous image, could indeed be called
 micron sized and one would not be dishonest. However the importance of
 hollow nickel tube could be the *sine qua non* of the Rossi scheme.



 Rossi has a history in his revelations, at least back when he was in full
 fund-raising mode, of first providing a bit too much information
 (inadvertently) and then backtracking later to try to minimize the damage.



 Thus, we often see conflicting statements which can be rationalized if one
 understands the history of Rossi-speak.



 This tubule mystery could be an exemplary example of what I am talking
 about. But did he actually ever say it?



 *From:* Eric Walker



 Does anyone  have the citation for Rossi's nickel lattice having tubules?
 Cannot find it. But check this out.

  Yes, please.  If anyone has a reference to Rossi using nickel with
 tubules, nanotubules, nanohairs, etc., please provide it.  My
 understanding is that he uses micron-sized nickel powder, treated in some
 way, and rather than something nano-.  There are carbon nanotubes, of
 course, and Rossi, as far as anyone knows, does not use them.



 It's remarkably difficult to pin the precise details down and keep them
 pinned down.  They keep on moving around and morphing through some kind of
 process of entropy.





RE: EXTERNAL: RE: [Vo]:MIT Course Day 5 -- NiH Systems

2014-02-07 Thread Jones Beene
Ah. tubercles instead of tubules . Thanks Bob

 

 

From: Bob Higgins 

 

Rossi has stated that he starts with 10 micron sized particles (since
identified as a nickel powder produced from the carbonyl process), adds a
catalyst (widely believed to be a nanopowder of some kind), and processes
the mix in a way that leads to amplified tubercles on the surface.

 

A search of tubules will not find the reference, he used tubercles.

 

I have replicated the growth of tubercles by doing just what Rossi
described.  

 



Re: EXTERNAL: RE: [Vo]:MIT Course Day 5 -- NiH Systems

2014-02-07 Thread Bob Cook
Bob--Bob Cook here

Your comments are revealing.  I believe quantum systems that are big enough to 
handle the energy fractionation that Hagelstein identifies in his lectures are 
a requirement for any solid state nuclear reaction.  A thermal conductor to get 
the heat out is also necessary.  These two objectives are probably at the heart 
of Rossi's design. 

 Of course the Kim BEC theory may occur at discrete locations in the Ni 
creating new quantum systems during the reactor operation.  However maintaining 
such nice locations for months of operation for the BEC's to form is 
questionable.  

Bob
  - Original Message - 
  From: Bob Higgins 
  To: vortex-l@eskimo.com 
  Cc: Bob Higgins 
  Sent: Friday, February 07, 2014 7:43 AM
  Subject: Re: EXTERNAL: RE: [Vo]:MIT Course Day 5 -- NiH Systems


  Rossi has stated that he starts with 10 micron sized particles (since 
identified as a nickel powder produced from the carbonyl process), adds a 
catalyst (widely believed to be a nanopowder of some kind), and processes the 
mix in a way that leads to amplified tubercles on the surface.


  A search of tubules will not find the reference, he used tubercles.


  I have replicated the growth of tubercles by doing just what Rossi described. 
 Begin with micron scale nickel powder (from the carbonyl precipitate process), 
add a nanopowder, mix, and heat in an oven with cycling H2, Ar, O2 process gas. 
 The result is a porous structure of tubercles with nanowires growing from 
the surface.  I suspect that both the nanowires and the tubercle structure are 
indicators that I am using similar processing of the powder mix as Rossi, but 
are not themselves the LENR NAE.  The observation is that when processed in 
that manner, there are plenty of NAE somewhere.  It is easy to believe that 
this structure (from the SEM pictures) will be rife with nanocracks as Dr. 
Storms suggests for the NAE.  In fact, the NAE are likely to be features you 
cannot see under the SEM rather than the features you can see.


  Bob Higgins



  On Fri, Feb 7, 2014 at 10:12 AM, Jones Beene jone...@pacbell.net wrote:

As Eric realizes, this is a critical issue for anyone wanting to replicated 
Rossi.



In fact, the material shown in the previous image, could indeed be called 
micron sized and one would not be dishonest. However the importance of hollow 
nickel tube could be the sine qua non of the Rossi scheme.



Rossi has a history in his revelations, at least back when he was in full 
fund-raising mode, of first providing a bit too much information 
(inadvertently) and then backtracking later to try to minimize the damage.



Thus, we often see conflicting statements which can be rationalized if one 
understands the history of Rossi-speak. 



This tubule mystery could be an exemplary example of what I am talking 
about. But did he actually ever say it?



From: Eric Walker 



  Does anyone  have the citation for Rossi's nickel lattice having 
tubules?
  Cannot find it. But check this out.

Yes, please.  If anyone has a reference to Rossi using nickel with 
tubules, nanotubules, nanohairs, etc., please provide it.  My 
understanding is that he uses micron-sized nickel powder, treated in some way, 
and rather than something nano-.  There are carbon nanotubes, of course, and 
Rossi, as far as anyone knows, does not use them.




It's remarkably difficult to pin the precise details down and keep them 
pinned down.  They keep on moving around and morphing through some kind of 
process of entropy.





Re: EXTERNAL: RE: [Vo]:MIT Course Day 5 -- NiH Systems

2014-02-07 Thread Bob Cook
Fran--

I agree fully.

Bob Cook
  - Original Message - 
  From: Roarty, Francis X 
  To: vortex-l@eskimo.com 
  Sent: Friday, February 07, 2014 5:36 AM
  Subject: RE: EXTERNAL: RE: [Vo]:MIT Course Day 5 -- NiH Systems


  IMHO grain size and geometry of these other alloys as powders will have a 
major effect on their LENR activity.

  Fran

   

  From: Jones Beene [mailto:jone...@pacbell.net] 
  Sent: Thursday, February 06, 2014 5:16 PM
  To: vortex-l@eskimo.com
  Subject: EXTERNAL: RE: [Vo]:MIT Course Day 5 -- NiH Systems

   

  From: Jed Rothwell 

   

  Superior for what? Conducting protons? Surely not for loading hydrogen. I 
have never heard that.

   

  Surely you read Ahern's Arata replication for EPRI ? 

   

  He achieved better loading than the standard of 1:1 with nickel-palladium 
alloy (at low Pd ratio in the alloy).

   

  Many alloys which are tailored for hydrogen storage are in fact better than 
palladium for that single property (which is the atomic ratio of lattice atoms 
to hydrogen atoms)

   

  This does not meant they will be more active for LENR - only that they will 
absorb more atoms of hydrogen per atom of lattice. That is what they are 
designed for.

   

  In fact, the alloys which store the most hydrogen are most often NOT 
anomalous as to energy release, when further stimulated. Unfortunately, the two 
fields have not been systematically investigated for determining the best of 
both worlds.

   

  Jones


Re: EXTERNAL: RE: [Vo]:MIT Course Day 5 -- NiH Systems

2014-02-07 Thread Bob Higgins
I believe that some fractionation must be taking place, but not to phonons.
 Phonons are contra-indicated by the experimental evidence.  Phonons
dissipate rapidly to heat with a decay constant that is based on the
acoustic velocity.  This means that the temperature will be extremely high
near the nanoscale NAE, making it much higher temperature than the bulk of
the reactor.  It suggests that before any useful total heat is realized for
the system, the NAE would burn itself out - melt, evaporate, etc.

On the other hand, if the output from the NAE was fractionated to lower
energy photons, then the decay constant would be based on the speed of
light in the material and the deposition to heat would be spread much
farther away from the NAE, allowing heat transport out of the NAE without
overheating the NAE structure.

The micro-explosions that have been reported are on a micron-scale, not on
a nano-scale; nanoscale would be expected with phonons.  The whole device
melt-downs that have been reported can only happen if the NAE is not that
much hotter than the bulk of the device.  Photons would spread the heat
away from the NAE in such a way that the meltdowns and micron-size
explosions could occur.

Keep in mind that Dr. Hagelstein has PRESUMED coupling to phonons in the
formulation of his mathematical experiment.  The formulation is not the
completely general case with the best solution popping out.  The general
formulation is too complex to solve today, so simplifying presumptions must
be made, and then the solutions are evaluated for consistency with
experiment.  The simplified formulation just makes it solve-able, not easy
to solve.  So, in this sense, Dr. Hagelstein is constructing mathematical
experiments (the simplifications) and is testing the solutions to see if
they match all of the experimental data.  If he guesses right in his
simplification (didn't leave out something important in his formulation),
and finds a match to all of the experimental data, then he has a good
theory.  It is all based on the same original physics which cannot be
solved in purely general form for the complex condensed matter environment.
 We may not know enough about the NAE to be able to simulate it today
because we don't know what simplifications are appropriate.

Bob


On Fri, Feb 7, 2014 at 12:54 PM, Bob Cook frobertc...@hotmail.com wrote:

  Bob--Bob Cook here

 Your comments are revealing.  I believe quantum systems that are big
 enough to handle the energy fractionation that Hagelstein identifies in his
 lectures are a requirement for any solid state nuclear reaction.  A thermal
 conductor to get the heat out is also necessary.  These two objectives are
 probably at the heart of Rossi's design.

  Of course the Kim BEC theory may occur at discrete locations in the Ni
 creating new quantum systems during the reactor operation.  However
 maintaining such nice locations for months of operation for the BEC's to
 form is questionable.

 Bob





Re: EXTERNAL: RE: [Vo]:MIT Course Day 5 -- NiH Systems

2014-02-07 Thread Eric Walker
On Fri, Feb 7, 2014 at 6:53 AM, Jones Beene jone...@pacbell.net wrote:

Does anyone  have the citation for Rossi’s nickel lattice having “tubules”?
 Cannot find it. But check this out.


Yes, please.  If anyone has a reference to Rossi using nickel with
tubules, nanotubules, nanohairs, etc., please provide it.  My
understanding is that he uses micron-sized nickel powder, treated in some
way, and rather than something nano-.  There are carbon nanotubes, of
course, and Rossi, as far as anyone knows, does not use them.

It's remarkably difficult to pin the precise details down and keep them
pinned down.  They keep on moving around and morphing through some kind of
process of entropy.

Eric


Re: EXTERNAL: RE: [Vo]:MIT Course Day 5 -- NiH Systems

2014-02-07 Thread Eric Walker
On Fri, Feb 7, 2014 at 7:43 AM, Bob Higgins rj.bob.higg...@gmail.comwrote:

Rossi has stated that he starts with 10 micron sized particles (since
 identified as a nickel powder produced from the carbonyl process), adds a
 catalyst (widely believed to be a nanopowder of some kind), and processes
 the mix in a way that leads to amplified tubercles on the surface.


Thanks for the helpful clarification.  I didn't realize that.  The main
reference I have found is Hank Mills's PESN article [1].  I'm curious where
Mills got this information.

It sounds like you have made a lot of progress on getting an NiH reactor
set up.  Have you seen anything interesting?

Eric


[1]
http://pesn.com/2012/01/02/9601998_Defkalion_Claims_No_Problem_with_Revealing_Cold_Fusion_Catalyst/