Re: [Biofuel] Pump size

2005-12-09 Thread Joe Street
Thanks Jim;

That IS a help.  As far as the actual mixing goes there must be big 
variances from one design of pump to another , in just what type of 
impeller is used and how close the tolerances are.  For my part I find 
my pump mixes things up very nicely in fact I can see the change in 
color through the plastic lines from the inlet to the outlet side of the 
pump.  The darker colour on the line that returns to the tank indicates 
the reaction is taking place.  I use a combination of vacuum and the 
pump inlet suction to pull the methoxide into the stream and have a 
needle valve on the methoxide line so that I set it up to introduce a 
slow trickle of methoxide into the stream entering the pump.  It takes 
me about 1/2 hour to add 4 liters of methoxide to 25 liters of oil.  I 
run the pump for a further 1/2 hour but I can see glycerine in the lower 
sight tube collecting even before the end of the first 1/2 hour.  So 
assuming my pump delivers 4 GPM  or 16 lpm I am doing roughly 16 changes 
in the time it takes to add the methoxide and then a further 16 changes 
after it is all added.  Someone questioned whether my little pump can do 
5 GPM through 3/8 inch lines and I suspect they may be right.  I should 
test it.  But even if it was only 2 GPM I would still be getting 16 
changes of volume in an hour which would still be above your 10 changes 
guideline.  BTW I'm curious to know the experience of those out there 
doing pump mixing for a longer term than me.  Does anyone find that the 
methoxide is chewing up your pump?

Joe



JJJN wrote:

Hi Joe,
The Clearwater Model 01479 is rated at 330 gallons per hour or 1249 
Liters per Hour when it has to lift Water no more than 0 foot before 
expelling it. It will lift water as much as 10 feet but you can expect 
the GPH or LPH to drop exponentially when you approach that much lift..

It will also take water in at 0 feet and expel it 115 feet but again you 
can expect it to drop exponentially when you get close to its Maximum.

That said,  lets review the purpose of the pump in the process.  The 
pump should do the mixing. This should be done as fast as possible (in 
an hour) as this is what gets the reaction going and the sooner we can 
start pulling the Glycerin off  thus pushing the reaction in the right 
direction.

So it is mixing we want to happen.  When we have a 25 gallon (94 L) 
batch and we place the Pump near the bottom or center of the reactor we 
can use 300 GPH as we are not lifting more than a foot or so and 
expelling the same and it is a round number.  So 300 / 25 = 12 (per 
hour) This theroreticaly is the number of times each liter passes 
through the pump in one hour. I personally like this number as my 
personal rule of thumb (10 time minimum and 2 extras to be sure)  If you 
get cheap here you will have oil unexposed to the Potassium Methoxil and 
end up with unreacted oil. I'm sorry I don't have a better rule for Max 
Min here but this is what I like to stick with.

Now if you go to the hardware store and buy a bag full of SSteel washers 
another of 1 PVC Couplings, 4 tees and 4 elbows you can increase the 
efficiency of the mix rate by building an orifice chamber like the one 
noted on JtF (Cambridge University) without increasing the restriction 
(4 runs minimum) the hole in the washer should be almost a half inch but 
it has to fit in the coupling.  This gadget will not work as well with 
out something to oscillate the oil but it will improve mixing 50% or so 
of what goes through the pump vers just the pipe and pump impeller.  One 
thing to remember is this just helps what goes through the pump.  The 
trick is get the whole batch through the pump!

You can also help this if you have a cone bottom reactor and you point 
the discharge hose so the oil in the reactor starts to circle around. 
This is pushing the top oil to the bottom (or through the pump). BUT USE 
CARE you dont want it creating a whirl pool!  just get it moving around 
nice and slow.

I hope this helps you some but again this is just what I have gleaned 
from the chemical engineers at work and I'm not sure they fully 
understand the biodiesel that I am absorbed with but the advice works 
for me.

Good Luck
Jim

Joe Street wrote:

  

Hi all;

I looked in the archives for info on pump size recommendations.  I found 
a few messages relating to the clear water pump but what I am after is 
does anyone have a rule of thumb on pump throughput versus reactor 
size?  I know variables such as reactor dimensions, tall vs short 
location of ports etc will have an impact but is there a ball park gauge 
such as GPM rating should be equal to some multiple or fraction of tank 
volume?  For example I have an 8 gallon tank and am using a pump which 
delivers 5 GPM at near zero head (unrestricted flow).  It works very 
well.  Does this mean that a 50 GPM pump would be a reasonable guess for 
a reactor of 80 gallons volume?  Keith you indicated that the clear 
water pump is ok for a 60 

Re: [Biofuel] Pump size

2005-12-09 Thread Michael Luich
Thanks Jim some good info, but I couldn't find the building an orifice chamber you mentioned on the JTF website.
Could you provide a link?

ThanksMichael LuichNow if you go to the hardware store and buy a bag full of SSteel washers
another of 1 PVC Couplings, 4 tees and 4 elbows you can increase theefficiency of the mix rate by building an orifice chamber like the onenoted on JtF (Cambridge University) without increasing the restriction
(4 runs minimum) the hole in the washer should be almost a half inch butit has to fit in the coupling.This gadget will not work as well without something to oscillate the oil but it will improve mixing 50% or so
of what goes through the pump vers just the pipe and pump impeller.Onething to remember is this just helps what goes through the pump.Thetrick is get the whole batch through the pump!

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[Biofuel] Pump size

2005-12-09 Thread Rumen Slavov
Hi Joe,Hi Jim,
  My reactor is pump mixed too,but I am using two
pumps of different types-one SS from the food brand
and the other is clear water-cast iron case and
turbine.As far I am controlling carefully the both and
I didn't`t noticed any changes,the pumps are in fine
condition.BTW,the pumps are capable of recirculating
the volume of the R 20-22 times in an hour and the BD
is prima!I tried for comparison injecting the MeOH in
the inlet and to pore slowly on the top and did not
noticed any diff in the BD-it is always OK.It seems
that the temp and agitation are what counts.
  Best
  Rumen

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Re: [Biofuel] Pump size

2005-12-09 Thread JJJN
Michael,
Here are the links,
http://www.cheng.cam.ac.uk/news/resnews/ChemEInterfaces6.pdf
http://www.cheng.cam.ac.uk/news/2004/biodiesel.html

I use a 1 dia PVC Coupling and a ss washer that just fits inside. the 
hole in the washer is about 1/2dia.

Jim


Michael Luich wrote:

 Thanks Jim some good info, but I couldn't find the building an 
 orifice chamber you mentioned on the JTF website.
 Could you provide a link?

 Thanks
 Michael Luich


 Now if you go to the hardware store and buy a bag full of SSteel
 washers
 another of 1 PVC Couplings, 4 tees and 4 elbows you can increase the
 efficiency of the mix rate by building an orifice chamber like the one
 noted on JtF (Cambridge University) without increasing the
 restriction
 (4 runs minimum) the hole in the washer should be almost a half
 inch but
 it has to fit in the coupling.  This gadget will not work as well with
 out something to oscillate the oil but it will improve mixing 50%
 or so
 of what goes through the pump vers just the pipe and pump
 impeller.  One
 thing to remember is this just helps what goes through the pump.  The
 trick is get the whole batch through the pump!





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Re: [Biofuel] Pump size

2005-12-08 Thread Keith Addison
Hi Joe

How come you're so metrically challenged? You're a Canadian, not an 
American, no? Cross-border pollution by sheer osmosis? LOL!

Hi all;

I looked in the archives for info on pump size recommendations.  I found
a few messages relating to the clear water pump but what I am after is
does anyone have a rule of thumb on pump throughput versus reactor
size?  I know variables such as reactor dimensions, tall vs short
location of ports etc will have an impact but is there a ball park gauge
such as GPM rating should be equal to some multiple or fraction of tank
volume?  For example I have an 8 gallon tank and am using a pump which
delivers 5 GPM at near zero head (unrestricted flow).  It works very
well.  Does this mean that a 50 GPM pump would be a reasonable guess for
a reactor of 80 gallons volume?  Keith you indicated that the clear
water pump is ok for a 60 gallon size

60 litres, about 16 US gallons.

but questionable for a 80 gallon size.

I think 100 litres is about the maximum, about 26 US gallons. It 
works at 60, 80 and probably 100 litres, and it doesn't work at 200 
litres (55 gal), or at least not as usually implemented. There are 
probably some work-arounds for that, but I reckon the best 
work-around would be a bigger pump.

Just to make things more confusing, the data on harbour freight's web
page says the 1 clear pump delivers 330 GPH so that's 5.5 GPM but it is
a 1/2 hp pump!

It's confusing. Harbor Freight says Maximum capacity: 330 GPH, 
Northern Tools says Moves up to 720 GPH at 2ft./10 GPM, whatever 
that means, same pump.

I find it's faster than 10 gpm, and that's with the thing stepped 
down from 1 to 3/4. Turning over 72 litres (oil plus methanol), 19 
US gallons, takes the pump less than 2 minutes. But that's not quite 
what happens, some gets more turned over than other.

My little pump is something like 1/20 hp and has 3/8
connections so there must be an error somewhere here.  I am thinking the
clear pump is actually 330 GPM not GPH.

No way!

I think the variable is the head. Would it be right to say that a 
biodiesel processor would be rather optimal conditions for a pump?

I don't know an easy way of calculating the variables to match a 
given reactor to a standard process and processing time. What people 
seem to do is to try to get in the ballpark and then use the fuel 
quality tests to fine-tune it. With stirrers there's the speed, the 
shape and configuration of the paddles, and you can use baffles. With 
pumps? Not so easy, you've gone and bought the thing already and 
rigged it to your processor, doing bracketing tests or something with 
different pumps isn't exactly an appealing option. So I can see why 
you'd want a rule-of-thumb, but I don't think there is one, sad to 
say, hope I'm wrong.

We managed to get it right first time, big relief, especially as I'd 
never built anything like a biodiesel reactor before. All it needed 
was a bit of tinkering with the plumbing, I didn't have to change 
anything. What we had was limited space, the 90-litre tanks and the 
pump, non-negotiables. I spent a lot of time reading Prof. Michael 
Allen's processor page at our site and his list posts and emails, and 
those of Camillo Holecek, and Michael's paper and spreadsheet on The 
modelling of the biodiesel reaction in our Biofuels library, along 
with anything else I could find, lots of list archives posts from 
lots of people.

I also spent quite a lot of time puzzling over the elevation of the 
outlet port. I was really pleased that that aspect of it in 
particular works well, I think it's a much neglected aspect of 
processing. See:
http://journeytoforever.org/biodiesel_processor10.html#settle

Along with the process itself, it might have quite a lot to do with 
this: How do you manage to make such clean biodiesel out of waste 
oil? a puzzled GC technician asked Midori in Tokyo yesterday at the 
university lab that's doing tests for us. It said so on the test 
results too in a comment at the end: Very clean biodiesel!!

We have some other test results of biodiesel made in one of the 
rather useless $70,000-and-up 100-litre processors these companies 
flog here in Japan, which the guy who bought it paid for at a 
professional lab ($6,000!). It didn't come close, although the test 
sample was taken *after* he'd centrifuged the finished, washed 
product and got a whole load of under-processed gunk out of it. I 
have some photographs of that, yuk. The other processor brands are 
the same, samples of their fuel don't pass the homebrewers' quality 
tests. The government issues warnings to people applying for the 
vegetable oil fuel exemption for the shaken (roadworthy 
certificate) to beware of poor-quality biodiesel, but it's the only 
kind you can buy. Don't buy biodiesel in Japan! Our processor cost 
$100. I'm not happy to tell you all this, I really wish these fancy 
processors could produce a fancy product but they can't. If we can do 
it, why can't they? The growing band of 

Re: [Biofuel] Pump size

2005-12-08 Thread JJJN
Hi Joe,
The Clearwater Model 01479 is rated at 330 gallons per hour or 1249 
Liters per Hour when it has to lift Water no more than 0 foot before 
expelling it. It will lift water as much as 10 feet but you can expect 
the GPH or LPH to drop exponentially when you approach that much lift..

It will also take water in at 0 feet and expel it 115 feet but again you 
can expect it to drop exponentially when you get close to its Maximum.

That said,  lets review the purpose of the pump in the process.  The 
pump should do the mixing. This should be done as fast as possible (in 
an hour) as this is what gets the reaction going and the sooner we can 
start pulling the Glycerin off  thus pushing the reaction in the right 
direction.

So it is mixing we want to happen.  When we have a 25 gallon (94 L) 
batch and we place the Pump near the bottom or center of the reactor we 
can use 300 GPH as we are not lifting more than a foot or so and 
expelling the same and it is a round number.  So 300 / 25 = 12 (per 
hour) This theroreticaly is the number of times each liter passes 
through the pump in one hour. I personally like this number as my 
personal rule of thumb (10 time minimum and 2 extras to be sure)  If you 
get cheap here you will have oil unexposed to the Potassium Methoxil and 
end up with unreacted oil. I'm sorry I don't have a better rule for Max 
Min here but this is what I like to stick with.

Now if you go to the hardware store and buy a bag full of SSteel washers 
another of 1 PVC Couplings, 4 tees and 4 elbows you can increase the 
efficiency of the mix rate by building an orifice chamber like the one 
noted on JtF (Cambridge University) without increasing the restriction 
(4 runs minimum) the hole in the washer should be almost a half inch but 
it has to fit in the coupling.  This gadget will not work as well with 
out something to oscillate the oil but it will improve mixing 50% or so 
of what goes through the pump vers just the pipe and pump impeller.  One 
thing to remember is this just helps what goes through the pump.  The 
trick is get the whole batch through the pump!

You can also help this if you have a cone bottom reactor and you point 
the discharge hose so the oil in the reactor starts to circle around. 
This is pushing the top oil to the bottom (or through the pump). BUT USE 
CARE you dont want it creating a whirl pool!  just get it moving around 
nice and slow.

I hope this helps you some but again this is just what I have gleaned 
from the chemical engineers at work and I'm not sure they fully 
understand the biodiesel that I am absorbed with but the advice works 
for me.

Good Luck
Jim

Joe Street wrote:

Hi all;

I looked in the archives for info on pump size recommendations.  I found 
a few messages relating to the clear water pump but what I am after is 
does anyone have a rule of thumb on pump throughput versus reactor 
size?  I know variables such as reactor dimensions, tall vs short 
location of ports etc will have an impact but is there a ball park gauge 
such as GPM rating should be equal to some multiple or fraction of tank 
volume?  For example I have an 8 gallon tank and am using a pump which 
delivers 5 GPM at near zero head (unrestricted flow).  It works very 
well.  Does this mean that a 50 GPM pump would be a reasonable guess for 
a reactor of 80 gallons volume?  Keith you indicated that the clear 
water pump is ok for a 60 gallon size but questionable for a 80 gallon size.
Just to make things more confusing, the data on harbour freight's web 
page says the 1 clear pump delivers 330 GPH so that's 5.5 GPM but it is 
a 1/2 hp pump!  My little pump is something like 1/20 hp and has 3/8 
connections so there must be an error somewhere here.  I am thinking the 
clear pump is actually 330 GPM not GPH.

Anybody?

Joe


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[Biofuel] Pump size

2005-12-07 Thread Joe Street
Hi all;

I looked in the archives for info on pump size recommendations.  I found 
a few messages relating to the clear water pump but what I am after is 
does anyone have a rule of thumb on pump throughput versus reactor 
size?  I know variables such as reactor dimensions, tall vs short 
location of ports etc will have an impact but is there a ball park gauge 
such as GPM rating should be equal to some multiple or fraction of tank 
volume?  For example I have an 8 gallon tank and am using a pump which 
delivers 5 GPM at near zero head (unrestricted flow).  It works very 
well.  Does this mean that a 50 GPM pump would be a reasonable guess for 
a reactor of 80 gallons volume?  Keith you indicated that the clear 
water pump is ok for a 60 gallon size but questionable for a 80 gallon size.
Just to make things more confusing, the data on harbour freight's web 
page says the 1 clear pump delivers 330 GPH so that's 5.5 GPM but it is 
a 1/2 hp pump!  My little pump is something like 1/20 hp and has 3/8 
connections so there must be an error somewhere here.  I am thinking the 
clear pump is actually 330 GPM not GPH.

Anybody?

Joe


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Re: [Biofuel] Pump size

2005-12-07 Thread Zeke Yewdall
What is the pressure that those gpm ratings are taken at?  I suspect
the 1/2 horse pump is rated at a much higher head than your 1/20th HP
pump.

Also, are you sure you are getting 5gpm through a 3/8 fitting?  It
seems a little high for that small of pipe.

On 12/7/05, Joe Street [EMAIL PROTECTED] wrote:
 Hi all;

 I looked in the archives for info on pump size recommendations.  I found
 a few messages relating to the clear water pump but what I am after is
 does anyone have a rule of thumb on pump throughput versus reactor
 size?  I know variables such as reactor dimensions, tall vs short
 location of ports etc will have an impact but is there a ball park gauge
 such as GPM rating should be equal to some multiple or fraction of tank
 volume?  For example I have an 8 gallon tank and am using a pump which
 delivers 5 GPM at near zero head (unrestricted flow).  It works very
 well.  Does this mean that a 50 GPM pump would be a reasonable guess for
 a reactor of 80 gallons volume?  Keith you indicated that the clear
 water pump is ok for a 60 gallon size but questionable for a 80 gallon size.
 Just to make things more confusing, the data on harbour freight's web
 page says the 1 clear pump delivers 330 GPH so that's 5.5 GPM but it is
 a 1/2 hp pump!  My little pump is something like 1/20 hp and has 3/8
 connections so there must be an error somewhere here.  I am thinking the
 clear pump is actually 330 GPM not GPH.

 Anybody?

 Joe


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Re: [Biofuel] Pump size

2005-12-07 Thread ufdaland
 I am thinking the 
clear pump is actually 330 GPM not GPH.

Joe , I just bought a 3/4 HP submersable and the well driller says it
will put out 10 GPM
Jerry

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Re: [biofuel] pump size

2004-09-03 Thread Appal Energy


Pierre,

Use what you tools you have and adjust your reaction time accordingly.

If the manufacturer's specs are available to you, check the rated gph of the
pump at 3' of head pressure. Then multiply that volume by ~60% due to
reductions caused by pumping a fluid far more viscous than water, which is
what the specs will probably refer to. Divide that volume by the volume in
the reactor and you've got a very crude guestimate of the number of
turnovers per hour in your reactor.

To judge an appropriate reaction time, pull an exact amount of fluid (200 ml
would suffice) out of the reaction stream every half-hour or hour after an
arbitrary initial ~1 hour reaction period.

Presuming that the contents of the reactor are kept homogenous from the pump
flow, the volume of the glycerol cocktail that settles out of each sample
will give you a fair gauge as to when your reaction completed.

The suggestion would be to continue the reaction for ~1/2 hour beyond the
point where your glyc cocktail volume stabilized.

Todd Swearingen

- Original Message - 
From: [EMAIL PROTECTED]
To: biofuel@yahoogroups.com
Sent: Thursday, September 02, 2004 5:26 PM
Subject: [biofuel] pump size


 Between all the exchange between some of our members, I lost sight
 of the ideal pump size  strength for mixing a 45 gallon drum of
 home brew (filled to 30 gal)

 Right now I have a 1/3 horse 1 pump. I am about to connect to my
 reactor.

 Is this in-/overly/perfectly adequate?


 Pierre





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[biofuel] pump size

2004-09-02 Thread pivincent

Between all the exchange between some of our members, I lost sight 
of the ideal pump size  strength for mixing a 45 gallon drum of 
home brew (filled to 30 gal)

Right now I have a 1/3 horse 1 pump. I am about to connect to my 
reactor.

Is this in-/overly/perfectly adequate?


Pierre




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