My third attempt:

Electrodes about 1.5" apart, instead of 1".

This time, I left it alone for about 50 minutes. The positive
electrode's surface started to turn gray after at least 20 minutes,
like it was being etched a little. The negative electrode began to 
accumulate silver fuzzies *very slowly*. 

At the end, I was able to carefully remove the negative electrode
without leaving any of the "fuzz" in the water.

The preparation is entirely colorless. 

So, there's no way of knowing what I've got without making some kind
of measurement?

Is there any way to test the concentration of silver in these
solutions? Some kind of titration? Like add a drop of this, add a
drop of something else as an indicator, and add drops of
whatchmacallit until it turns color?

Just a crude go/no go check to make sure you have at least something 
in suspension, and not way too much would be fine by me.

Anyway, get the variables worked out once, and not much is going to 
change. But how do you get it calibrated?

I suppose some of you went through this nit-picky phase until you 
decided it's just not that important. :-)

Thanks to Marsha, Donna, and others for their encouragement!

Mike
[Mike Devour, Citizen, Patriot, Libertarian]
[[email protected]                       ]
[Speaking only for himself...              ]