Hi Brian,

Thanks for the input.  Yes, it depends on how the search was performed.  I
tested with out specifying the mass for a SILAC sample and it seemed to
work.  If you have different mass labels for heavy and light and the light
is not specified as a static mod then you have to do what you showed in
your commandline.  Ultimately, it is always a good idea to verify for
yourself that the masses it uses are the correct ones.


Cheers,
-David

On Tue, Jun 12, 2012 at 1:08 PM, Brian Hampton <[email protected]> wrote:

> David,
>
> I am doing very similar work as Alex where light and heavy labels are on K
> and the N-terminus of the peptides.  In the Tandem parameters file, the
> modifications are specified according the the API description from Tandem
> for residue modification mass and allows to search with two different
> labels on the same residue.
>
> residue, modification mass Lightmod@K, Lightmod@[
> residue, potential modification mass Heavymod-Lightmod@K,
> Heavymod-Lightmod@[
> In my case Lightmod=42.024 and Heavymod=48.028
>
> In ASAPRatio,  if I do not specify a modification mass (as you seem to
> suggest below) for the amino acids it matches up the pairs incorrectly.
>  Rather than finding labeled pairs of peptides differing by 6u, it finds
> light labeled and *unlabeled* pairs differing by 42u, which doesn't exist.
>
> So I specify n and K in the "Change modified residues to" since the
> N-terminus and K are the only labeled residues and then I specify all four
> labeled residue masses with their respective monoisotopic masses of 42 & 48
> for n and 170.0124 and 170.0125 for K.  Then it seems to work.  Maybe it
> works differently with input from another search engine, I don't know.
>
> I am guessing the following warning is informational only and doesn't
> indicate something is wrong:
>
> running: "/usr/local/apps/tpp/bin/ASAPRatioPeptideParser 
> 'BH_2-interact.pep.xml' -lnK -b -r0.5 -mn42.024n48.028K170.0124K176.0125"
> WARNING: Found more than one variable mod on 'K'. Please make sure to specify 
> a heavy mass for this residue.
>
> Thanks in advance for any help here.
>
> Brian
>
>
> On Mon, Jun 11, 2012 at 4:02 PM, David Shteynberg <
> [email protected]> wrote:
>
>> Hi Alex,
>>
>> If your tandem search used monoisotopic masses for the variable mods then
>> you don't really have to specify the masses and it will use the mass in the
>> file.  ASAPRatio allows you to redefine the mass (so you can use average
>> masses for matching fragments and monoisotopic for quantitation), if the
>> pep.xml file alread has the monoisotopic masses listed then you can just
>> specify the labeled amino acids and those will be applied to find the
>> heavy/light pairs.  Let me know if you require further clarification.
>>
>> Cheers,
>> -David
>>
>> On Mon, Jun 11, 2012 at 12:47 PM, Alex <[email protected]> wrote:
>>
>>> Quick question, probably directed to David,
>>>
>>> I've used ASAPratio by following through a couple of posts, trying to
>>> figure out how to complete the options on Petunia. It still remains a
>>> little unclear why or what should be completed in the fields:
>>> Change labeled residues to
>>> Specified residue mass 1:
>>> I work with dimethylated labels (formaldehyde reagent targeting free
>>> amino groups and its 'heavy' deuterated D2CO form) and  understand I should
>>> add K and n as the "change labeled residues" and add the mass of the heavy
>>> residues to the "specified residue mass" (n=33.06425 and K=160.15137 for
>>> the deuterium modified labels). This has so far worked out to me.
>>>
>>> My question is why should they be added to both fields? Is this
>>> redundant or is there any case where one could add a modification to one
>>> field and not the other? I have added all the modifications (light and
>>> heavy labels) to the X!Tandem parameters files, including other modifs as
>>> alkylated cystesines and oxidized M and all the peptides have been
>>> correctly identified. Judging by the previous posts, this has caused
>>> confusion to other ASAPratio users in the past.
>>>
>>> And a suggestion: it would be very convenient to have a 'zoom' and
>>> 'unzoom' option when viewing the results on the ASAPratio viewer.
>>> Sometimes, ASAPratio offers a very narrow window of the integrated peak,
>>> and I find viewing the axis in a larger window is good to assess how
>>> specific the XIC looks for a particular precursor along the complete
>>> chromtographic run.
>>>
>>> Thanks TTP people, hope to hearing back from you!!!
>>>
>>> Alex
>>>
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