What are the usual titrations on your oil blend?  Also, what is your batch
success?  I think that eth processing is very interesting to many people
and this info would be appreciated.

Thanks,

James Slayden

On Wed, 15 Jan 2003, Ken Provost wrote:

> 
> On Wednesday, January 15, 2003, at 10:02  AM, James Slayden wrote:
> 
> > I noticed the 5:1 eth:meth ratio both on JTF and in your postings. 
> > Since
> > your doing the "kicker" of meth after the initial reaction, might it
> > just
> > be better to up the meth in meth/eth oxide mix, to something like
> > 3:1?  How much meth are you adding in the kicker phase to the whole
> > reaction?  Also, are you using WVO or crude oil.  I thought I remember
> > a
> > posting just recently that you had various drums of oil in your garage,
> > and something about salad .....  ;-)
> 
> I believe the kicker functions differently than if the same amount of
> total methanol were included from the beginning. The first phase
> with ethanol and methanol allows the equilibrium to go as far as it can
> without glycerine separation, and allows the ethanol time to react
> which seems slower than the methanol reaction. The kicker is
> specifically intended to initiate separation, which pulls the
> equilibrium
> the rest of the way. Amounts are detailed in my write-up.
> 
> I haven't rigorously investigated this, because it's rather difficult.
> One
> would have to find just the right combination of the right ingredients
> such that you could get separation using the kicker approach, but not
> if you put in all the methanol up front. In other words, there are many
> more examples where the result is negative than there are where it's
> positive. In the absence of proof, I just adopt the method that seems
> sensible and leave the rigor to others :-)
> 
> My oil is a mix of WVO  and flush oil, selecting from sesame, olive, and
> 


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