tom davis wrote:

>In making testbatches of biodiesel, what safety precautions need to 
>be taken to protect yourself from the sodium methoxide and the gases 
>generated from the reaction?  Do I need gas masks or just a cloth 
>mask anything to keep the fumes out of my eyes and lungs?

If you start here:

"Where do I start?"
http://journeytoforever.org/biodiesel_make.html#start

... (and you should) you'll find plenty of safety advice as you go along.

For instance:

>Organic vapor cartridge respirators are more or less useless against 
>methanol vapors. Professional advice is not to use organic vapor 
>cartridges for longer than a few hours maximum, or not to use them 
>at all. Only a supplied-air system will do (SCBA -- Self-Contained 
>Breathing Apparatus).
>
>The best advice is not to expose yourself to the fumes in the first 
>place. The main danger is when the methanol is hot -- when it's cold 
>or at "room temperature" it fumes very little, and this is easily 
>avoided. Don't use "open" reactors -- biodiesel processors should be 
>closed to the atmosphere, with no fumes escaping. All methanol 
>containers should be kept tightly closed anyway to prevent water 
>absorption from the air.
>
>We transfer methanol from its container to the methoxide mixing 
>container by pumping it, with no exposure at all. This is easily 
>arranged, and an ordinary aquarium air-pump will do (the same one 
>you use for washing the biodiesel). The methoxide is mixed like this 
>-- Methoxide the easy way, which also happens to be the safe way. 
>The mixture gets quite hot at first, but the container is kept 
>closed and no fumes escape. When mixed, the methoxide is again 
>pumped into the (closed) biodiesel processor with the aquarium 
>air-pump -- there's no exposure to fumes, and it's added slowly, 
>which is optimal for the process and also for safety. See Adding the 
>methoxide.

It's all hot-linked, everything you need, including details on safe 
test-batch processors.

Best wishes

Keith



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