On Sep 2, 2010, at 9:34 PM, jimlux wrote:
> maybe 1E-6 micron (1E-9 torr)..

Maybe that's closer to what it was, and I just misremembered the value. It's 
been a long time, and that was my only experience with high vacuum equipment.

> Sounds about right.. the mechanical pump will pull it down to a few microns 
> in a minute or so (I assume it's like a bell jar with maybe 50 liters total 
> volume?)

As I recall, there was a machined stainless steel lid with a glass viewing port 
over the evaporation chamber, then a large bell jar lowered over that. The 
heating filament was pretty substantial, and we'd run around a hundred amps 
through it as I recall, controlled by dialing up a large variac while watching 
a current meter. The filament was near the bottom of the chamber, with a 
perforated stainless steel plate over it. We'd place the wafers to be plated 
face-down over holes in that plate, and also set a glass slide in a designated 
spot on that plate. The viewing port allowed the filament to be viewed through 
the glass slide, and we'd control the amount of metal to be deposited by 
turning off the heat once the glowing filament was no longer visible through 
the metal deposited onto the glass slide.

As a side effect, the used glass slides made nice gold- or aluminum-plated 
first-surface mirrors. Rumor was that they'd recycle the glass and discard the 
gold, which was too thin to be worth salvaging! That may be a tall tale, though.

> Lots of interlocks to keep you from doing dumb stuff (e.g. venting to 
> atmosphere with the diff pump hot and connected), actually not all that 
> dirty.. you probably weren't sticking complex mechanical stuff in there.. 
> basically a wafer that you'd put next to the evaporator source.  So no issues 
> with virtual leaks, etc.

Yes, just a few wafers and a glass slide on the perforated plate, and a small 
bit of metal wire on the filament. We weren't burdened with maintaining the 
machine (aside from topping up the LN trap), but I'd guess that the teaching 
assistant would have to clean the chamber occasionally, i.e. to remove goopy 
photoresist residue from the perforated plate. I don't know whether the 
evaporator was made on-site or purchased, but I would guess that it was made 
on-site.


> At work, we've got tons (well, tens) of these little evaporation workstation 
> things.. A rolling cart about a meter by half a meter, and a meter high, with 
> a bell jar on top.  A mechanical two stage pump and a 3" diff pump under the 
> plate.  A couple of feedthroughs for current to heat the evaporation source.  
> A couple toggle switches, a ion and a thermocouple gage..  We don't use the 
> for evaporating metal (at least I and the folks in my section don't)... we 
> use them to test electronics under vacuum..

Cool. It'd be funny if the cleaning crew surreptitiously plated their hubcaps 
and stuff late at night...



-- 
Mark J. Blair, NF6X <[email protected]>
Web page: http://www.nf6x.net/
GnuPG public key available from my web page.





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