Proces to produce nickel from Nickel Carbonyl:

http://en.wikipedia.org/wiki/Mond_process





On Fri, Aug 23, 2013 at 9:54 PM, Axil Axil <[email protected]> wrote:

> I might be wrong. The are a large amount of "light elements" present. You
> may be totally correct.:
>
>
> On Fri, Aug 23, 2013 at 3:48 PM, Axil Axil <[email protected]> wrote:
>
>> Re:
>>
>> TABLE II
>>
>> XRF ANALYSIS OF NAE5 (BEFORE A TEST RUN)
>>
>> TEST ID: 07/18/12 #25
>>
>> From the composition of the powder from the ICCF-17 DGT paper, no carbon
>> is present.
>>
>>
>> On Fri, Aug 23, 2013 at 3:44 PM, Axil Axil <[email protected]> wrote:
>>
>>> Thanks, I stand corrected. I see what you mean. They must remove the
>>> carbon with oxygen and then the oxygen with hydrogen starting from the
>>> commercial powder..
>>>
>>> The presence of carbon will distort (increase) the curie temperature of
>>> the powder. Therefore, Carbon must be removed.
>>>
>>>
>>> On Fri, Aug 23, 2013 at 3:30 PM, Bob Higgins 
>>> <[email protected]>wrote:
>>>
>>>> The micrograph is of carbonyl Ni.  Look it up.  For example, Hunter
>>>> Chemical AH50.  Also, Vale T255.  It is the same as what is shown in Kim's
>>>> slides.  Carbonyl is the process - the particles are pure Ni.
>>>>  On Aug 23, 2013 3:25 PM, "Axil Axil" <[email protected]> wrote:
>>>>
>>>>> DGT has never mentioned the use of  carbonyl. There powder is pure
>>>>> nickel. The surface of the particles are processed with a proprietary
>>>>> process to resurface the particle with a Rutile structure.
>>>>>
>>>>> Please show me a reference to the use of  carbonyl in this process.
>>>>> In fact, the use of carbonyl is incompatible with  the rutile process.
>>>>>
>>>>>
>>>>> On Fri, Aug 23, 2013 at 3:00 PM, Bob Higgins <[email protected]
>>>>> > wrote:
>>>>>
>>>>>> Yes.  What is shown is a carbonyl Ni particle.  It has no nanowires.
>>>>>> It does have points, but no nanowires.  Nanowires would not be visible at
>>>>>> the scale of that micrograph.
>>>>>> On Aug 23, 2013 2:29 PM, "Axil Axil" <[email protected]> wrote:
>>>>>>
>>>>>>> Are you looking at slide 3, fabrication of fuels and reaction cells?
>>>>>>>
>>>>>>> the box of interest starts with the following...
>>>>>>>
>>>>>>> Modified Ni Crystal powders....
>>>>>>>
>>>>>>> The 5 micron particle is pictured on that page. Can you see it now...
>>>>>>>
>>>>>>>
>>>>>>> On Fri, Aug 23, 2013 at 1:58 PM, Bob Higgins <
>>>>>>> [email protected]> wrote:
>>>>>>>
>>>>>>>> The carbony Ni particles used by DGT, as was shown in Kim's
>>>>>>>> presentation, have NO nanowires at all.
>>>>>>>>
>>>>>>>>
>>>>>>>> On Fri, Aug 23, 2013 at 1:33 PM, Axil Axil <[email protected]>wrote:
>>>>>>>>
>>>>>>>>> Not for the first time, with amazing generosity, DGT has provided
>>>>>>>>> us with a picture of a 5 micron nanowire coated micro-particle in 
>>>>>>>>> their
>>>>>>>>> ICCF-18 presentation that they have originally engineered base on 
>>>>>>>>> suggested
>>>>>>>>> information derived from Rossi’s revelations.
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>> There must be a million nanowires coming off that fuzzy looking
>>>>>>>>> micro-particle.
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>> If 10 nanoparticle aggregation form on each nanowire tip and 100
>>>>>>>>> hot spots from inside each aggregation, that drive the NAE count for 
>>>>>>>>> each
>>>>>>>>> micro-particle up to 10 to the power of 9 hot spots per 
>>>>>>>>> micro-particle.
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>> If 10,000,000 micro particles as used in the 3 grams of nickel
>>>>>>>>> power reaction activator, then the NAE count goes up to 10 to the 16 
>>>>>>>>> power
>>>>>>>>> of possible NAE sites in a Ni/H reactor.
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>> Clearly, this micro-powder covered with nanowires approach to the
>>>>>>>>> reaction has many orders of magnitude numerical superiority over the 
>>>>>>>>> crack
>>>>>>>>> regime.
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>>
>>>>>>>>> On Fri, Aug 23, 2013 at 12:06 PM, Edmund Storms <
>>>>>>>>> [email protected]> wrote:
>>>>>>>>>
>>>>>>>>>> Peter, I'm simply telling you what your comments mean to me. I'm
>>>>>>>>>> not thinking in your place. If I have gotten the wrong understanding 
>>>>>>>>>> from
>>>>>>>>>> what you have written, than you are free to tell me and to correct 
>>>>>>>>>> your
>>>>>>>>>> writings so that other people do not also get the wrong impression, 
>>>>>>>>>> which
>>>>>>>>>> is clearly the case.
>>>>>>>>>>
>>>>>>>>>> I do not think a crack is equally active along its length. I'm
>>>>>>>>>> only proposing that somewhere in the gap, the fusion reaction is 
>>>>>>>>>> possible.
>>>>>>>>>> I have described ALL aspects of the model. I'm only giving the broad
>>>>>>>>>> requirements. Once these are accepted, you will be told more 
>>>>>>>>>> details.  I
>>>>>>>>>> see no reason to waste my time if the basic claim is rejected. I 
>>>>>>>>>> would
>>>>>>>>>> rather spend my time using the model to make the effect work.
>>>>>>>>>>
>>>>>>>>>> Ed
>>>>>>>>>> On Aug 23, 2013, at 9:53 AM, Peter Gluck wrote:
>>>>>>>>>>
>>>>>>>>>> Dear Ed.
>>>>>>>>>>
>>>>>>>>>> I would ask you to not think in my place, I really don't like
>>>>>>>>>> it.It is typical for dictatures and I had enough from it starting 
>>>>>>>>>> with
>>>>>>>>>> :"Der Fuhrer denkt fur uns alle" and ending with Ceausescu's 
>>>>>>>>>> omniscience. I
>>>>>>>>>> have the right to think independently.
>>>>>>>>>> Citing you:
>>>>>>>>>> *you are assuming that D+Pd involves a different mechanism, a
>>>>>>>>>> different NAE, and different nuclear products. *
>>>>>>>>>> Clearly the products of reaction are different for Pd and Ni H
>>>>>>>>>> simply because
>>>>>>>>>> the reactants are different. I have NOT told that the mechanism
>>>>>>>>>> of reaction
>>>>>>>>>> are different.
>>>>>>>>>> A question for you- a crack however beautiful is inherently very
>>>>>>>>>> asymmetric
>>>>>>>>>> do you think a crack nanometers broad but microns or even
>>>>>>>>>> millimeters long
>>>>>>>>>> is equally active along its entire lengths? Isn't it more
>>>>>>>>>> plausible that inside
>>>>>>>>>> this labyrinthic formation there are some even more preferential
>>>>>>>>>> short areas
>>>>>>>>>> where the activity is focused? And are you convinced that thse
>>>>>>>>>> short areas
>>>>>>>>>> are so different from a nanostructure? Couldn't be the things a
>>>>>>>>>> bit more
>>>>>>>>>> complicated but actually more unitary- as you otherwise also
>>>>>>>>>> suggest?
>>>>>>>>>>
>>>>>>>>>> I think it is not possible to decide now sitting at our PC's if
>>>>>>>>>> Nature uses
>>>>>>>>>> only one soltion or more for creating excess energy. It is more
>>>>>>>>>> useful
>>>>>>>>>> to find new ways to force Nature to give us what we need and want
>>>>>>>>>> and not care so much if she is whining a bit for that.
>>>>>>>>>>
>>>>>>>>>> Peter
>>>>>>>>>>
>>>>>>>>>>
>>>>>>>>>> On Fri, Aug 23, 2013 at 6:16 PM, Edmund Storms <
>>>>>>>>>> [email protected]> wrote:
>>>>>>>>>>
>>>>>>>>>>>
>>>>>>>>>>> On Aug 23, 2013, at 9:03 AM, Peter Gluck wrote:
>>>>>>>>>>>
>>>>>>>>>>> Dear Bob,
>>>>>>>>>>>
>>>>>>>>>>> Thank you for the idea of cracks' aesthetics! I know it well, I
>>>>>>>>>>> think
>>>>>>>>>>> you have remarked the second Motto by Leonard Cohen based
>>>>>>>>>>>  on this idea..
>>>>>>>>>>> It happens that very early in my professional career I learned
>>>>>>>>>>> about the
>>>>>>>>>>> beauty and variety of cracks -when working at the Civil
>>>>>>>>>>> Engineering
>>>>>>>>>>> Faculy of the Timisoara- Polytechnics, Chair of Concrete. It is
>>>>>>>>>>> a world of cracks in concrete see e.g.
>>>>>>>>>>> http://indecorativeconcrete.com/idcn/wp-content/uploads/2012/02/Why-Concrete-Cracks.pdf
>>>>>>>>>>> Mistery and beauty are different from function. Let's admit the
>>>>>>>>>>> possible role
>>>>>>>>>>> cracks in Pd in the FPCell, is this something good for the
>>>>>>>>>>> results?
>>>>>>>>>>> However Paintelli's process is based on very smart and beautiful
>>>>>>>>>>> nanostructures more sophisticated and educated as cracks, and LENR+ 
>>>>>>>>>>> uses
>>>>>>>>>>> the high art of nanoplasmonics.
>>>>>>>>>>>
>>>>>>>>>>>
>>>>>>>>>>> How do you know this Peter?  Besides, you are assuming that D+Pd
>>>>>>>>>>> involves a different mechanism, a different NAE, and different 
>>>>>>>>>>> nuclear
>>>>>>>>>>> products. Consequently, the number of miracles is squared rather 
>>>>>>>>>>> than
>>>>>>>>>>> reduced. Do you really want to go down that path? What happens the 
>>>>>>>>>>> effect
>>>>>>>>>>> occurs using Ti?  Does this involve an additional method and 
>>>>>>>>>>> mechanism?
>>>>>>>>>>>  What how is tritium formed? Is this reaction different in Ni 
>>>>>>>>>>> compared to
>>>>>>>>>>> Pd?
>>>>>>>>>>>
>>>>>>>>>>>  I believe the phenomenon is so rare and unusual that only one
>>>>>>>>>>> condition and mechanism would be able to cause it. You take the 
>>>>>>>>>>> opposite
>>>>>>>>>>> view, that every material and isotope requires a different method 
>>>>>>>>>>> and NAE.
>>>>>>>>>>>  This gives people a choice. I wonder how the vote would go?
>>>>>>>>>>>
>>>>>>>>>>> Ed
>>>>>>>>>>>
>>>>>>>>>>>
>>>>>>>>>>> Peter
>>>>>>>>>>>
>>>>>>>>>>> ,
>>>>>>>>>>>
>>>>>>>>>>>
>>>>>>>>>>> On Fri, Aug 23, 2013 at 5:05 PM, Bob Higgins <
>>>>>>>>>>> [email protected]> wrote:
>>>>>>>>>>>
>>>>>>>>>>>> Recently, Peter published in his blog his reasons for hoping
>>>>>>>>>>>> that the NAE aren’t cracks. After considering it, I believe he 
>>>>>>>>>>>> misses the
>>>>>>>>>>>> uniqueness, durability, and beauty of the cracks that are being 
>>>>>>>>>>>> considered.
>>>>>>>>>>>> ****
>>>>>>>>>>>>
>>>>>>>>>>>> ** **
>>>>>>>>>>>>
>>>>>>>>>>>> To the uniqueness point…  Consider that a crack is different
>>>>>>>>>>>> than just two surfaces in close proximity. A crack is like a horn 
>>>>>>>>>>>> with a
>>>>>>>>>>>> throat of minimum gap: the lattice spacing.  Imagine the throat at 
>>>>>>>>>>>> x=0 with
>>>>>>>>>>>> the crack surface spacing widening as x increases.  The crack 
>>>>>>>>>>>> provides a
>>>>>>>>>>>> unique environment in its smallest regions.  Near x=0, the 
>>>>>>>>>>>> environment for
>>>>>>>>>>>> a hydron asymptotically approaches that of the lattice.  In this 
>>>>>>>>>>>> region,
>>>>>>>>>>>> electron orbitals extend across or at least into the crack.  
>>>>>>>>>>>> Perhaps in
>>>>>>>>>>>> this near-lattice spacing there is only room for an H+ ion (the 
>>>>>>>>>>>> case for
>>>>>>>>>>>> Ni, but for Pd there is room at the lattice spacing for a neutral 
>>>>>>>>>>>> monatomic
>>>>>>>>>>>> hydron).  As x increases, the crack surface spacing (the gap) 
>>>>>>>>>>>> increases
>>>>>>>>>>>> allowing room for neutral monatomic hydrons.  At greater x, the 
>>>>>>>>>>>> crack
>>>>>>>>>>>> spacing would support neutral H2 molecules, and beyond this, the 
>>>>>>>>>>>> crack is
>>>>>>>>>>>> probably uninteresting.  This unique gradient of hydron boundary 
>>>>>>>>>>>> conditions
>>>>>>>>>>>> always exists in the crack near it throat (near x=0), even if the 
>>>>>>>>>>>> crack
>>>>>>>>>>>> were to begin zipping itself open.****
>>>>>>>>>>>>
>>>>>>>>>>>> ** **
>>>>>>>>>>>>
>>>>>>>>>>>> To the durability point…  In my past I had occasion to work
>>>>>>>>>>>> with MEMS structures.  When I first saw MEMS cantilever beams 
>>>>>>>>>>>> being used
>>>>>>>>>>>> for switches and other functions, my first thought was, “Those are 
>>>>>>>>>>>> going to
>>>>>>>>>>>> break!”  What I learned was that a structure’s strength is 
>>>>>>>>>>>> inversely
>>>>>>>>>>>> proportional to its size.  So a building scaled twice as large 
>>>>>>>>>>>> will be half
>>>>>>>>>>>> as strong.  This is why you can drop an ant from as high as you 
>>>>>>>>>>>> wish and he
>>>>>>>>>>>> will hit the ground running.  Compare a 3 meter diving board 
>>>>>>>>>>>> (cantilever)
>>>>>>>>>>>> to a 3 micron cantilever – the 3 micron cantilever will be a 
>>>>>>>>>>>> million times
>>>>>>>>>>>> more robust.  The cracks being considered for NAE are nanoscale 
>>>>>>>>>>>> cracks, but
>>>>>>>>>>>> our natural experience is with cracks having dimensions of ~1cm.  
>>>>>>>>>>>> A 10nm
>>>>>>>>>>>> crack, will be a million times more mechanically robust than a 1cm 
>>>>>>>>>>>> crack.
>>>>>>>>>>>> At the nanoscale, the two split apart surfaces will be very stiff 
>>>>>>>>>>>> and
>>>>>>>>>>>> behind the throat of the crack (x<0) there will be compression 
>>>>>>>>>>>> forces
>>>>>>>>>>>> trying to restore the crack to its closed position.  The surfaces 
>>>>>>>>>>>> may also
>>>>>>>>>>>> experience a Casimir closing force.  A nanoscale crack will have 
>>>>>>>>>>>> strong
>>>>>>>>>>>> forces trying to heal itself.****
>>>>>>>>>>>>
>>>>>>>>>>>> ****
>>>>>>>>>>>>
>>>>>>>>>>>> If nanocracks can heal, then how would the nanocrack form in
>>>>>>>>>>>> the first place and what could keep the surfaces apart?  I believe 
>>>>>>>>>>>> a wedge
>>>>>>>>>>>> of atom(s) or molecule(s) is needed in the gap to keep the crack 
>>>>>>>>>>>> open, and
>>>>>>>>>>>> perhaps to form it in the first place.  That is why I am using
>>>>>>>>>>>> nanoparticles that will alloy with Ni and then I am oxidizing the
>>>>>>>>>>>> structure.  I use iron oxide nanoparticles.  I put down the oxide
>>>>>>>>>>>> nanoparticles disposed all across the Ni micro-powder surface, 
>>>>>>>>>>>> reduce (or
>>>>>>>>>>>> partly reduce) the surface so the iron nanoparticles can alloy 
>>>>>>>>>>>> with the Ni,
>>>>>>>>>>>> and then go back and strongly oxidize the metals.  When the iron 
>>>>>>>>>>>> oxidizes,
>>>>>>>>>>>> it grows in volume and I hypothesize that it will wedge open a 
>>>>>>>>>>>> nanocrack.
>>>>>>>>>>>> If the iron is then partly reduced it becomes an H2 splitting 
>>>>>>>>>>>> catalyst,
>>>>>>>>>>>> right at the site of the crack.****
>>>>>>>>>>>>
>>>>>>>>>>>> ** **
>>>>>>>>>>>>
>>>>>>>>>>>> What a beautiful structure I imagine that to be – a nanocrack
>>>>>>>>>>>> with a sweep of hydron boundary conditions with an H2 splitting 
>>>>>>>>>>>> catalyst at
>>>>>>>>>>>> its mouth.****
>>>>>>>>>>>>
>>>>>>>>>>>> ** **
>>>>>>>>>>>>
>>>>>>>>>>>> Bob****
>>>>>>>>>>>>
>>>>>>>>>>>
>>>>>>>>>>>
>>>>>>>>>>>
>>>>>>>>>>> --
>>>>>>>>>>> Dr. Peter Gluck
>>>>>>>>>>> Cluj, Romania
>>>>>>>>>>> http://egooutpeters.blogspot.com
>>>>>>>>>>>
>>>>>>>>>>>
>>>>>>>>>>>
>>>>>>>>>>
>>>>>>>>>>
>>>>>>>>>> --
>>>>>>>>>> Dr. Peter Gluck
>>>>>>>>>> Cluj, Romania
>>>>>>>>>> http://egooutpeters.blogspot.com
>>>>>>>>>>
>>>>>>>>>>
>>>>>>>>>>
>>>>>>>>>
>>>>>>>>
>>>>>>>
>>>>>
>>>
>>
>

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