Re: [Biofuel] Crude fatty acid distillate

2007-01-26 Thread tanuki
Jan / James,

You've been good help!!  I'm going to do some tests this coming week.
Thanks so much!!  Any other inputs are still welcome!!

best regards,

Ken

- Original Message -
From: JAMES PHELPS [EMAIL PROTECTED]
To: biofuel@sustainablelists.org
Sent: Thursday, January 25, 2007 2:53 AM
Subject: Re: [Biofuel] Crude fatty acid distillate


 Jan, Ken,
 I have pushed the procedure to double the acid amount in the first phase,
 dewatered and went to the second phase (base base) in small batches
without
 problem.  I suggest testing in small amounts and working up a procedure
that
 fits the product. This will take some time to do but when you get it you
 can get repeatbility thereafter.  I did use Venturi acid introduction so
 that perhaps makes a big difference as well.

 Jim


 From: Jan Warnqvist [EMAIL PROTECTED]
 Reply-To: biofuel@sustainablelists.org
 To: biofuel@sustainablelists.org
 Subject: Re: [Biofuel] Crude fatty acid distillate
 Date: Wed, 24 Jan 2007 12:48:10 +0100
 
 If you have that much tri-glycerides you may most likely do one acid
 esterification followed by one base trans-esterification. Just check the
 FFA
 value after the first step after removal of the (acidic) water phase. If
 the
 FFA value is  5%, go as described above, in any other case as described
 before.
 With best regards
 AGERATEC AB
 Jan Warnqvist
 - Original Message -
 From: [EMAIL PROTECTED]
 To: biofuel@sustainablelists.org
 Sent: Wednesday, January 24, 2007 10:02 AM
 Subject: Re: [Biofuel] Crude fatty acid distillate
 
 
   Thanks again Jan.
  
   Its 71.8% FFA.  But doing acid esterification twice? Do you finish
with
 a
   base transesterification after the two acid esterification?
   Please pardon my ignorance.  Can you expound a bit.  First time to
hear
   about acid esterification twice.  Appreciate very much your help on
the
   matter.
  
   Thanks.
  
   Ken
  
   - Original Message -
   From: Jan Warnqvist [EMAIL PROTECTED]
   To: biofuel@sustainablelists.org
   Sent: Tuesday, January 23, 2007 4:46 PM
   Subject: Re: [Biofuel] Crude fatty acid distillate
  
  
   No, if you are working with 100% free fatty acids, you will have to
do
   the
   ACID esterification twice with water content evapoation inbetween
  
   With best regards
   AGERATEC AB
   Jan Warnqvist.
   - Original Message -
   From: [EMAIL PROTECTED]
   To: biofuel@sustainablelists.org
   Sent: Tuesday, January 23, 2007 9:22 AM
   Subject: Re: [Biofuel] Crude fatty acid distillate
  
  
Thanks Jan,
   
So you are saying that Aleks Kac's two stage process is the way to
go
on
this one?  Start with the acid-based stage and finish with the
   base-based
stage.  That's doing it twice right?
   
Am doing small batches on the single stage base process (about 100
   liters
veg. oil).  Will blending this with new veg. oil make a difference?
   
Been reading the Foolproof Method over and over again to
familiarize
myself.
Looks like it.
   
Much thanks again.
   
Ken
   
- Original Message -
From: Jan Warnqvist [EMAIL PROTECTED]
To: biofuel@sustainablelists.org
Sent: Tuesday, January 23, 2007 3:35 PM
Subject: Re: [Biofuel] Crude fatty acid distillate
   
   
Hello Ken,
fatty acids are possible to esterify with an acid catalyst. The
 formed
water
has to be drawn off, so it is always nice to start with a low
water
content.
Performed correctly, the esterification will produce 90-95%
esters.
Usually
these kinds of reactions are performed twice for a good conversion
   grade.
   
With best regards
AGERATEC AB
Jan Warnqvist
- Original Message -
From: [EMAIL PROTECTED]
To: biofuel@sustainablelists.org
Sent: Tuesday, January 23, 2007 8:18 AM
Subject: Re: [Biofuel] Crude fatty acid distillate
   
   
 Hi everyone,

 I sent this out a few days ago.  I was told by someone in the
oil
   mill
 that
 crude fatty acid distillate is just a fancy name for their
seconds
 or
 reject
 oils, which soap factories take from them and make into soap.
 Anyone
has
 any experience with this kind of stock being made into
biodiesel?
   Will
 such
 a high FFA content give problems?

 Thanks.

 Ken


 - Original Message -
 From: [EMAIL PROTECTED]
 To: Biofuel@sustainablelists.org
 Sent: Thursday, January 18, 2007 10:15 AM
 Subject: [Biofuel] Crude fatty acid distillate


 Hi everyone,

 An oil mill has just told me that they have excess of crude
fatty
   acid
 distillate which they can give me with the following
 specifications
   :

 Free Fatty Acid (As Lauric)  -  71.8%
 Iodine Value mg I/g  - 10
 Total Fatty Matter- 96%
 Moisture  Impurities   - 0.5%
 Saponifiable Value mg KOH/g   -  260
 Unsaponifiable Matter

Re: [Biofuel] Crude fatty acid distillate

2007-01-24 Thread tanuki
Thanks again Jan.

Its 71.8% FFA.  But doing acid esterification twice? Do you finish with a
base transesterification after the two acid esterification?
Please pardon my ignorance.  Can you expound a bit.  First time to hear
about acid esterification twice.  Appreciate very much your help on the
matter.

Thanks.

Ken

- Original Message -
From: Jan Warnqvist [EMAIL PROTECTED]
To: biofuel@sustainablelists.org
Sent: Tuesday, January 23, 2007 4:46 PM
Subject: Re: [Biofuel] Crude fatty acid distillate


 No, if you are working with 100% free fatty acids, you will have to do the
 ACID esterification twice with water content evapoation inbetween

 With best regards
 AGERATEC AB
 Jan Warnqvist.
 - Original Message -
 From: [EMAIL PROTECTED]
 To: biofuel@sustainablelists.org
 Sent: Tuesday, January 23, 2007 9:22 AM
 Subject: Re: [Biofuel] Crude fatty acid distillate


  Thanks Jan,
 
  So you are saying that Aleks Kac's two stage process is the way to go on
  this one?  Start with the acid-based stage and finish with the
base-based
  stage.  That's doing it twice right?
 
  Am doing small batches on the single stage base process (about 100
liters
  veg. oil).  Will blending this with new veg. oil make a difference?
 
  Been reading the Foolproof Method over and over again to familiarize
  myself.
  Looks like it.
 
  Much thanks again.
 
  Ken
 
  - Original Message -
  From: Jan Warnqvist [EMAIL PROTECTED]
  To: biofuel@sustainablelists.org
  Sent: Tuesday, January 23, 2007 3:35 PM
  Subject: Re: [Biofuel] Crude fatty acid distillate
 
 
  Hello Ken,
  fatty acids are possible to esterify with an acid catalyst. The formed
  water
  has to be drawn off, so it is always nice to start with a low water
  content.
  Performed correctly, the esterification will produce 90-95% esters.
  Usually
  these kinds of reactions are performed twice for a good conversion
grade.
 
  With best regards
  AGERATEC AB
  Jan Warnqvist
  - Original Message -
  From: [EMAIL PROTECTED]
  To: biofuel@sustainablelists.org
  Sent: Tuesday, January 23, 2007 8:18 AM
  Subject: Re: [Biofuel] Crude fatty acid distillate
 
 
   Hi everyone,
  
   I sent this out a few days ago.  I was told by someone in the oil
mill
   that
   crude fatty acid distillate is just a fancy name for their seconds or
   reject
   oils, which soap factories take from them and make into soap.  Anyone
  has
   any experience with this kind of stock being made into biodiesel?
Will
   such
   a high FFA content give problems?
  
   Thanks.
  
   Ken
  
  
   - Original Message -
   From: [EMAIL PROTECTED]
   To: Biofuel@sustainablelists.org
   Sent: Thursday, January 18, 2007 10:15 AM
   Subject: [Biofuel] Crude fatty acid distillate
  
  
   Hi everyone,
  
   An oil mill has just told me that they have excess of crude fatty
acid
   distillate which they can give me with the following specifications
:
  
   Free Fatty Acid (As Lauric)  -  71.8%
   Iodine Value mg I/g  - 10
   Total Fatty Matter- 96%
   Moisture  Impurities   - 0.5%
   Saponifiable Value mg KOH/g   -  260
   Unsaponifiable Matter-  0.32%
  
   I am now doing some small production for my own use with a blend of
   WVO
   and
   new oil on the single stage process.  I've read up on the two stage
   process
   and it looks like the above will take a two stage process with 71.8%
  FFA.
   Am I right?  Anyone out there with some thoughts on the matter?  Its
  free
   stuff for me although its only about 200liters monthly.  Would it be
   better
   to blend it or process it separately?
  
   Thanks
  
   Ken
  
  
   ___
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http://sustainablelists.org/mailman/listinfo/biofuel_sustainablelists.org
  
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http://sustainablelists.org/mailman/listinfo/biofuel_sustainablelists.org
  
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   Search the combined Biofuel and Biofuels-biz list archives (50,000
   messages):
   http://www.mail-archive.com/biofuel@sustainablelists.org/
  
  
  
 
 
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  Biofuel at Journey to Forever:
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  messages):
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Re: [Biofuel] Crude fatty acid distillate

2007-01-24 Thread JAMES PHELPS
Jan, Ken,
I have pushed the procedure to double the acid amount in the first phase, 
dewatered and went to the second phase (base base) in small batches without 
problem.  I suggest testing in small amounts and working up a procedure that 
fits the product. This will take some time to do but when you get it you 
can get repeatbility thereafter.  I did use Venturi acid introduction so 
that perhaps makes a big difference as well.

Jim


From: Jan Warnqvist [EMAIL PROTECTED]
Reply-To: biofuel@sustainablelists.org
To: biofuel@sustainablelists.org
Subject: Re: [Biofuel] Crude fatty acid distillate
Date: Wed, 24 Jan 2007 12:48:10 +0100

If you have that much tri-glycerides you may most likely do one acid
esterification followed by one base trans-esterification. Just check the 
FFA
value after the first step after removal of the (acidic) water phase. If 
the
FFA value is  5%, go as described above, in any other case as described
before.
With best regards
AGERATEC AB
Jan Warnqvist
- Original Message -
From: [EMAIL PROTECTED]
To: biofuel@sustainablelists.org
Sent: Wednesday, January 24, 2007 10:02 AM
Subject: Re: [Biofuel] Crude fatty acid distillate


  Thanks again Jan.
 
  Its 71.8% FFA.  But doing acid esterification twice? Do you finish with 
a
  base transesterification after the two acid esterification?
  Please pardon my ignorance.  Can you expound a bit.  First time to hear
  about acid esterification twice.  Appreciate very much your help on the
  matter.
 
  Thanks.
 
  Ken
 
  - Original Message -
  From: Jan Warnqvist [EMAIL PROTECTED]
  To: biofuel@sustainablelists.org
  Sent: Tuesday, January 23, 2007 4:46 PM
  Subject: Re: [Biofuel] Crude fatty acid distillate
 
 
  No, if you are working with 100% free fatty acids, you will have to do
  the
  ACID esterification twice with water content evapoation inbetween
 
  With best regards
  AGERATEC AB
  Jan Warnqvist.
  - Original Message -
  From: [EMAIL PROTECTED]
  To: biofuel@sustainablelists.org
  Sent: Tuesday, January 23, 2007 9:22 AM
  Subject: Re: [Biofuel] Crude fatty acid distillate
 
 
   Thanks Jan,
  
   So you are saying that Aleks Kac's two stage process is the way to go
   on
   this one?  Start with the acid-based stage and finish with the
  base-based
   stage.  That's doing it twice right?
  
   Am doing small batches on the single stage base process (about 100
  liters
   veg. oil).  Will blending this with new veg. oil make a difference?
  
   Been reading the Foolproof Method over and over again to familiarize
   myself.
   Looks like it.
  
   Much thanks again.
  
   Ken
  
   - Original Message -
   From: Jan Warnqvist [EMAIL PROTECTED]
   To: biofuel@sustainablelists.org
   Sent: Tuesday, January 23, 2007 3:35 PM
   Subject: Re: [Biofuel] Crude fatty acid distillate
  
  
   Hello Ken,
   fatty acids are possible to esterify with an acid catalyst. The 
formed
   water
   has to be drawn off, so it is always nice to start with a low water
   content.
   Performed correctly, the esterification will produce 90-95% esters.
   Usually
   these kinds of reactions are performed twice for a good conversion
  grade.
  
   With best regards
   AGERATEC AB
   Jan Warnqvist
   - Original Message -
   From: [EMAIL PROTECTED]
   To: biofuel@sustainablelists.org
   Sent: Tuesday, January 23, 2007 8:18 AM
   Subject: Re: [Biofuel] Crude fatty acid distillate
  
  
Hi everyone,
   
I sent this out a few days ago.  I was told by someone in the oil
  mill
that
crude fatty acid distillate is just a fancy name for their seconds
or
reject
oils, which soap factories take from them and make into soap.
Anyone
   has
any experience with this kind of stock being made into biodiesel?
  Will
such
a high FFA content give problems?
   
Thanks.
   
Ken
   
   
- Original Message -
From: [EMAIL PROTECTED]
To: Biofuel@sustainablelists.org
Sent: Thursday, January 18, 2007 10:15 AM
Subject: [Biofuel] Crude fatty acid distillate
   
   
Hi everyone,
   
An oil mill has just told me that they have excess of crude fatty
  acid
distillate which they can give me with the following 
specifications
  :
   
Free Fatty Acid (As Lauric)  -  71.8%
Iodine Value mg I/g  - 10
Total Fatty Matter- 96%
Moisture  Impurities   - 0.5%
Saponifiable Value mg KOH/g   -  260
Unsaponifiable Matter-  0.32%
   
I am now doing some small production for my own use with a blend 
of
WVO
and
new oil on the single stage process.  I've read up on the two 
stage
process
and it looks like the above will take a two stage process with
71.8%
   FFA.
Am I right?  Anyone out there with some thoughts on the matter?
Its
   free
stuff for me although its only about 200liters monthly.  Would it
be
better
to blend it or process it separately?
   
Thanks

Re: [Biofuel] Crude fatty acid distillate

2007-01-24 Thread Jan Warnqvist
Ken, the important thing is that you do the measurements necessary in order 
to decide how to proceed.

With best regards
AGERATEC AB
Jan Warnqvist
- Original Message - 
From: JAMES PHELPS [EMAIL PROTECTED]
To: biofuel@sustainablelists.org
Sent: Wednesday, January 24, 2007 7:53 PM
Subject: Re: [Biofuel] Crude fatty acid distillate


 Jan, Ken,
 I have pushed the procedure to double the acid amount in the first phase,
 dewatered and went to the second phase (base base) in small batches 
 without
 problem.  I suggest testing in small amounts and working up a procedure 
 that
 fits the product. This will take some time to do but when you get it you
 can get repeatbility thereafter.  I did use Venturi acid introduction so
 that perhaps makes a big difference as well.

 Jim


From: Jan Warnqvist [EMAIL PROTECTED]
Reply-To: biofuel@sustainablelists.org
To: biofuel@sustainablelists.org
Subject: Re: [Biofuel] Crude fatty acid distillate
Date: Wed, 24 Jan 2007 12:48:10 +0100

If you have that much tri-glycerides you may most likely do one acid
esterification followed by one base trans-esterification. Just check the
FFA
value after the first step after removal of the (acidic) water phase. If
the
FFA value is  5%, go as described above, in any other case as described
before.
With best regards
AGERATEC AB
Jan Warnqvist
- Original Message -
From: [EMAIL PROTECTED]
To: biofuel@sustainablelists.org
Sent: Wednesday, January 24, 2007 10:02 AM
Subject: Re: [Biofuel] Crude fatty acid distillate


  Thanks again Jan.
 
  Its 71.8% FFA.  But doing acid esterification twice? Do you finish with
a
  base transesterification after the two acid esterification?
  Please pardon my ignorance.  Can you expound a bit.  First time to hear
  about acid esterification twice.  Appreciate very much your help on the
  matter.
 
  Thanks.
 
  Ken
 
  - Original Message -
  From: Jan Warnqvist [EMAIL PROTECTED]
  To: biofuel@sustainablelists.org
  Sent: Tuesday, January 23, 2007 4:46 PM
  Subject: Re: [Biofuel] Crude fatty acid distillate
 
 
  No, if you are working with 100% free fatty acids, you will have to do
  the
  ACID esterification twice with water content evapoation inbetween
 
  With best regards
  AGERATEC AB
  Jan Warnqvist.
  - Original Message -
  From: [EMAIL PROTECTED]
  To: biofuel@sustainablelists.org
  Sent: Tuesday, January 23, 2007 9:22 AM
  Subject: Re: [Biofuel] Crude fatty acid distillate
 
 
   Thanks Jan,
  
   So you are saying that Aleks Kac's two stage process is the way to 
   go
   on
   this one?  Start with the acid-based stage and finish with the
  base-based
   stage.  That's doing it twice right?
  
   Am doing small batches on the single stage base process (about 100
  liters
   veg. oil).  Will blending this with new veg. oil make a difference?
  
   Been reading the Foolproof Method over and over again to familiarize
   myself.
   Looks like it.
  
   Much thanks again.
  
   Ken
  
   - Original Message -
   From: Jan Warnqvist [EMAIL PROTECTED]
   To: biofuel@sustainablelists.org
   Sent: Tuesday, January 23, 2007 3:35 PM
   Subject: Re: [Biofuel] Crude fatty acid distillate
  
  
   Hello Ken,
   fatty acids are possible to esterify with an acid catalyst. The
formed
   water
   has to be drawn off, so it is always nice to start with a low water
   content.
   Performed correctly, the esterification will produce 90-95% esters.
   Usually
   these kinds of reactions are performed twice for a good conversion
  grade.
  
   With best regards
   AGERATEC AB
   Jan Warnqvist
   - Original Message -
   From: [EMAIL PROTECTED]
   To: biofuel@sustainablelists.org
   Sent: Tuesday, January 23, 2007 8:18 AM
   Subject: Re: [Biofuel] Crude fatty acid distillate
  
  
Hi everyone,
   
I sent this out a few days ago.  I was told by someone in the oil
  mill
that
crude fatty acid distillate is just a fancy name for their 
seconds
or
reject
oils, which soap factories take from them and make into soap.
Anyone
   has
any experience with this kind of stock being made into biodiesel?
  Will
such
a high FFA content give problems?
   
Thanks.
   
Ken
   
   
- Original Message -
From: [EMAIL PROTECTED]
To: Biofuel@sustainablelists.org
Sent: Thursday, January 18, 2007 10:15 AM
Subject: [Biofuel] Crude fatty acid distillate
   
   
Hi everyone,
   
An oil mill has just told me that they have excess of crude 
fatty
  acid
distillate which they can give me with the following
specifications
  :
   
Free Fatty Acid (As Lauric)  -  71.8%
Iodine Value mg I/g  - 10
Total Fatty Matter- 96%
Moisture  Impurities   - 0.5%
Saponifiable Value mg KOH/g   -  260
Unsaponifiable Matter-  0.32%
   
I am now doing some small production for my own use with a blend
of
WVO
and
new oil on the single stage process

Re: [Biofuel] Crude fatty acid distillate

2007-01-23 Thread tanuki
Thanks Jan,

So you are saying that Aleks Kac's two stage process is the way to go on
this one?  Start with the acid-based stage and finish with the base-based
stage.  That's doing it twice right?

Am doing small batches on the single stage base process (about 100 liters
veg. oil).  Will blending this with new veg. oil make a difference?

Been reading the Foolproof Method over and over again to familiarize myself.
Looks like it.

Much thanks again.

Ken

- Original Message -
From: Jan Warnqvist [EMAIL PROTECTED]
To: biofuel@sustainablelists.org
Sent: Tuesday, January 23, 2007 3:35 PM
Subject: Re: [Biofuel] Crude fatty acid distillate


 Hello Ken,
 fatty acids are possible to esterify with an acid catalyst. The formed
water
 has to be drawn off, so it is always nice to start with a low water
content.
 Performed correctly, the esterification will produce 90-95% esters.
Usually
 these kinds of reactions are performed twice for a good conversion grade.

 With best regards
 AGERATEC AB
 Jan Warnqvist
 - Original Message -
 From: [EMAIL PROTECTED]
 To: biofuel@sustainablelists.org
 Sent: Tuesday, January 23, 2007 8:18 AM
 Subject: Re: [Biofuel] Crude fatty acid distillate


  Hi everyone,
 
  I sent this out a few days ago.  I was told by someone in the oil mill
  that
  crude fatty acid distillate is just a fancy name for their seconds or
  reject
  oils, which soap factories take from them and make into soap.  Anyone
has
  any experience with this kind of stock being made into biodiesel?  Will
  such
  a high FFA content give problems?
 
  Thanks.
 
  Ken
 
 
  - Original Message -
  From: [EMAIL PROTECTED]
  To: Biofuel@sustainablelists.org
  Sent: Thursday, January 18, 2007 10:15 AM
  Subject: [Biofuel] Crude fatty acid distillate
 
 
  Hi everyone,
 
  An oil mill has just told me that they have excess of crude fatty acid
  distillate which they can give me with the following specifications :
 
  Free Fatty Acid (As Lauric)  -  71.8%
  Iodine Value mg I/g  - 10
  Total Fatty Matter- 96%
  Moisture  Impurities   - 0.5%
  Saponifiable Value mg KOH/g   -  260
  Unsaponifiable Matter-  0.32%
 
  I am now doing some small production for my own use with a blend of WVO
  and
  new oil on the single stage process.  I've read up on the two stage
  process
  and it looks like the above will take a two stage process with 71.8%
FFA.
  Am I right?  Anyone out there with some thoughts on the matter?  Its
free
  stuff for me although its only about 200liters monthly.  Would it be
  better
  to blend it or process it separately?
 
  Thanks
 
  Ken
 
 
  ___
  Biofuel mailing list
  Biofuel@sustainablelists.org
 
http://sustainablelists.org/mailman/listinfo/biofuel_sustainablelists.org
 
  Biofuel at Journey to Forever:
  http://journeytoforever.org/biofuel.html
 
  Search the combined Biofuel and Biofuels-biz list archives (50,000
  messages):
  http://www.mail-archive.com/biofuel@sustainablelists.org/
 
 
  ___
  Biofuel mailing list
  Biofuel@sustainablelists.org
 
http://sustainablelists.org/mailman/listinfo/biofuel_sustainablelists.org
 
  Biofuel at Journey to Forever:
  http://journeytoforever.org/biofuel.html
 
  Search the combined Biofuel and Biofuels-biz list archives (50,000
  messages):
  http://www.mail-archive.com/biofuel@sustainablelists.org/
 
 
 


 ___
 Biofuel mailing list
 Biofuel@sustainablelists.org
 http://sustainablelists.org/mailman/listinfo/biofuel_sustainablelists.org

 Biofuel at Journey to Forever:
 http://journeytoforever.org/biofuel.html

 Search the combined Biofuel and Biofuels-biz list archives (50,000
messages):
 http://www.mail-archive.com/biofuel@sustainablelists.org/


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Re: [Biofuel] Crude fatty acid distillate

2007-01-23 Thread Jan Warnqvist
No, if you are working with 100% free fatty acids, you will have to do the 
ACID esterification twice with water content evapoation inbetween

With best regards
AGERATEC AB
Jan Warnqvist.
- Original Message - 
From: [EMAIL PROTECTED]
To: biofuel@sustainablelists.org
Sent: Tuesday, January 23, 2007 9:22 AM
Subject: Re: [Biofuel] Crude fatty acid distillate


 Thanks Jan,

 So you are saying that Aleks Kac's two stage process is the way to go on
 this one?  Start with the acid-based stage and finish with the base-based
 stage.  That's doing it twice right?

 Am doing small batches on the single stage base process (about 100 liters
 veg. oil).  Will blending this with new veg. oil make a difference?

 Been reading the Foolproof Method over and over again to familiarize 
 myself.
 Looks like it.

 Much thanks again.

 Ken

 - Original Message -
 From: Jan Warnqvist [EMAIL PROTECTED]
 To: biofuel@sustainablelists.org
 Sent: Tuesday, January 23, 2007 3:35 PM
 Subject: Re: [Biofuel] Crude fatty acid distillate


 Hello Ken,
 fatty acids are possible to esterify with an acid catalyst. The formed
 water
 has to be drawn off, so it is always nice to start with a low water
 content.
 Performed correctly, the esterification will produce 90-95% esters.
 Usually
 these kinds of reactions are performed twice for a good conversion grade.

 With best regards
 AGERATEC AB
 Jan Warnqvist
 - Original Message -
 From: [EMAIL PROTECTED]
 To: biofuel@sustainablelists.org
 Sent: Tuesday, January 23, 2007 8:18 AM
 Subject: Re: [Biofuel] Crude fatty acid distillate


  Hi everyone,
 
  I sent this out a few days ago.  I was told by someone in the oil mill
  that
  crude fatty acid distillate is just a fancy name for their seconds or
  reject
  oils, which soap factories take from them and make into soap.  Anyone
 has
  any experience with this kind of stock being made into biodiesel?  Will
  such
  a high FFA content give problems?
 
  Thanks.
 
  Ken
 
 
  - Original Message -
  From: [EMAIL PROTECTED]
  To: Biofuel@sustainablelists.org
  Sent: Thursday, January 18, 2007 10:15 AM
  Subject: [Biofuel] Crude fatty acid distillate
 
 
  Hi everyone,
 
  An oil mill has just told me that they have excess of crude fatty acid
  distillate which they can give me with the following specifications :
 
  Free Fatty Acid (As Lauric)  -  71.8%
  Iodine Value mg I/g  - 10
  Total Fatty Matter- 96%
  Moisture  Impurities   - 0.5%
  Saponifiable Value mg KOH/g   -  260
  Unsaponifiable Matter-  0.32%
 
  I am now doing some small production for my own use with a blend of 
  WVO
  and
  new oil on the single stage process.  I've read up on the two stage
  process
  and it looks like the above will take a two stage process with 71.8%
 FFA.
  Am I right?  Anyone out there with some thoughts on the matter?  Its
 free
  stuff for me although its only about 200liters monthly.  Would it be
  better
  to blend it or process it separately?
 
  Thanks
 
  Ken
 
 
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  messages):
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Re: [Biofuel] Crude fatty acid distillate

2007-01-22 Thread tanuki
Hi everyone,

I sent this out a few days ago.  I was told by someone in the oil mill that
crude fatty acid distillate is just a fancy name for their seconds or reject
oils, which soap factories take from them and make into soap.  Anyone has
any experience with this kind of stock being made into biodiesel?  Will such
a high FFA content give problems?

Thanks.

Ken


- Original Message -
From: [EMAIL PROTECTED]
To: Biofuel@sustainablelists.org
Sent: Thursday, January 18, 2007 10:15 AM
Subject: [Biofuel] Crude fatty acid distillate


 Hi everyone,

 An oil mill has just told me that they have excess of crude fatty acid
 distillate which they can give me with the following specifications :

 Free Fatty Acid (As Lauric)  -  71.8%
 Iodine Value mg I/g  - 10
 Total Fatty Matter- 96%
 Moisture  Impurities   - 0.5%
 Saponifiable Value mg KOH/g   -  260
 Unsaponifiable Matter-  0.32%

 I am now doing some small production for my own use with a blend of WVO
and
 new oil on the single stage process.  I've read up on the two stage
process
 and it looks like the above will take a two stage process with 71.8% FFA.
 Am I right?  Anyone out there with some thoughts on the matter?  Its free
 stuff for me although its only about 200liters monthly.  Would it be
better
 to blend it or process it separately?

 Thanks

 Ken


 ___
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 Biofuel@sustainablelists.org
 http://sustainablelists.org/mailman/listinfo/biofuel_sustainablelists.org

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 http://journeytoforever.org/biofuel.html

 Search the combined Biofuel and Biofuels-biz list archives (50,000
messages):
 http://www.mail-archive.com/biofuel@sustainablelists.org/


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Re: [Biofuel] Crude fatty acid distillate

2007-01-22 Thread Jan Warnqvist
Hello Ken,
fatty acids are possible to esterify with an acid catalyst. The formed water 
has to be drawn off, so it is always nice to start with a low water content. 
Performed correctly, the esterification will produce 90-95% esters. Usually 
these kinds of reactions are performed twice for a good conversion grade.

With best regards
AGERATEC AB
Jan Warnqvist
- Original Message - 
From: [EMAIL PROTECTED]
To: biofuel@sustainablelists.org
Sent: Tuesday, January 23, 2007 8:18 AM
Subject: Re: [Biofuel] Crude fatty acid distillate


 Hi everyone,

 I sent this out a few days ago.  I was told by someone in the oil mill 
 that
 crude fatty acid distillate is just a fancy name for their seconds or 
 reject
 oils, which soap factories take from them and make into soap.  Anyone has
 any experience with this kind of stock being made into biodiesel?  Will 
 such
 a high FFA content give problems?

 Thanks.

 Ken


 - Original Message -
 From: [EMAIL PROTECTED]
 To: Biofuel@sustainablelists.org
 Sent: Thursday, January 18, 2007 10:15 AM
 Subject: [Biofuel] Crude fatty acid distillate


 Hi everyone,

 An oil mill has just told me that they have excess of crude fatty acid
 distillate which they can give me with the following specifications :

 Free Fatty Acid (As Lauric)  -  71.8%
 Iodine Value mg I/g  - 10
 Total Fatty Matter- 96%
 Moisture  Impurities   - 0.5%
 Saponifiable Value mg KOH/g   -  260
 Unsaponifiable Matter-  0.32%

 I am now doing some small production for my own use with a blend of WVO
 and
 new oil on the single stage process.  I've read up on the two stage
 process
 and it looks like the above will take a two stage process with 71.8% FFA.
 Am I right?  Anyone out there with some thoughts on the matter?  Its free
 stuff for me although its only about 200liters monthly.  Would it be
 better
 to blend it or process it separately?

 Thanks

 Ken


 ___
 Biofuel mailing list
 Biofuel@sustainablelists.org
 http://sustainablelists.org/mailman/listinfo/biofuel_sustainablelists.org

 Biofuel at Journey to Forever:
 http://journeytoforever.org/biofuel.html

 Search the combined Biofuel and Biofuels-biz list archives (50,000
 messages):
 http://www.mail-archive.com/biofuel@sustainablelists.org/


 ___
 Biofuel mailing list
 Biofuel@sustainablelists.org
 http://sustainablelists.org/mailman/listinfo/biofuel_sustainablelists.org

 Biofuel at Journey to Forever:
 http://journeytoforever.org/biofuel.html

 Search the combined Biofuel and Biofuels-biz list archives (50,000 
 messages):
 http://www.mail-archive.com/biofuel@sustainablelists.org/


 


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[Biofuel] Crude fatty acid distillate

2007-01-17 Thread tanuki
Hi everyone,

An oil mill has just told me that they have excess of crude fatty acid
distillate which they can give me with the following specifications :

Free Fatty Acid (As Lauric)  -  71.8%
Iodine Value mg I/g  - 10
Total Fatty Matter- 96%
Moisture  Impurities   - 0.5%
Saponifiable Value mg KOH/g   -  260
Unsaponifiable Matter-  0.32%

I am now doing some small production for my own use with a blend of WVO and
new oil on the single stage process.  I've read up on the two stage process
and it looks like the above will take a two stage process with 71.8% FFA.
Am I right?  Anyone out there with some thoughts on the matter?  Its free
stuff for me although its only about 200liters monthly.  Would it be better
to blend it or process it separately?

Thanks

Ken


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