can increase the temperature of the
reaction mixture to cut down the time taken for the reaction as
ethanol boils at 78C rather than 65C, and if there are any other
hints/ tips people can give through their experience of this reaction.
Thanks
Charles List
of metal? Also, is the impeller in the
clearwater pump plastic? As I know you can get some with stainless
steel blades, I wonder my impeller break-up was due to age or chemicals.
Thanks
Charles List
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Tom
- Original Message -
From: Charles List [EMAIL PROTECTED]
To: biofuel@sustainablelists.org
Sent: Tuesday, June 20, 2006 5:25 PM
Subject: Re: [Biofuel] Help needed!
Hi Tom
Many thanks for the advice. I will let you know how I get on.
I intend (hopefully) to run B100
in there,
Tom
P.S.
What % biodiesel do you intend to burn in your boiler?
Any adjustments to the burner (pressure, nozzle, air flow?)
(Just curious)
- Original Message -
From: Charles List [EMAIL PROTECTED]
To: biofuel@sustainablelists.org
Sent: Monday, June 19
- Original Message -
From: Charles List [EMAIL PROTECTED]
To: biofuel@sustainablelists.org
Sent: Sunday, June 18, 2006 4:29 PM
Subject: Re: [Biofuel] Help needed!
Hi Tom
Thanks for that, I tried 70l at the weekend and end-product still
black, so I tried a 1l batch, still black!! I am using new
gallons, little
buggers show
up in the methanol sol. test).
Slow and methodical pays off.
Best of luck.
Let me know how it goes,
Tom
- Original Message -
From: Charles List [EMAIL PROTECTED]
To: biofuel
Message -
From: Charles List [EMAIL PROTECTED]
To: biofuel@sustainablelists.org
Sent: Wednesday, June 14, 2006 8:04 PM
Subject: Re: [Biofuel] Help needed!
Hi again
Unfortunately no-one has answered my last post- have I found an
insurmountable problem?!
Going back a few steps and trying
have trawled the archives but I can't seem to find anything that will
help. I realise that I have some incomplete reactions happening but
I am confused by the continually different results.
Charles
On 13/06/2006, at 8:30 AM, Charles List wrote:
Hi all
I have just scaled up to a 150l
used 150ml methanol and 5.8g 85% KOH as my
base amount on my test batch. Unfortunately nothing happened, 12
hours later, no separation, no split, no more glycerine! Has the
petrodiesel stuffed it up? What can I do?
Charles List
of further washing. They are talking about the ethanol
trans-esterification method, but I was wondering whether anyone had
tried this with the methanol method and could tell me how effective
it is.
Best Regards
Charles List
clear!
Regards
Charles List
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Hi NigelI'm in Alexandra in South Island and I'm struggling with getting methanol delivered- I seem to need a class 3 certification for the chemical companies to deliver any to me and no-one seems to know how I go about getting one!Any thoughts?CharlesOn 22/02/2006, at 2:28 PM, Nigel Kelly wrote:
YupHe's basically refluxing it, I assume, with the liebig condenser vertically attached to the reaction vessel. A closed container would do the same thing!A good use for the liebig condenser would be to reclaim the excess methanol from the glycerine, but they are usually pretty small, so would
Hi
Anyone out there from New Zealand who can tell me where to get
competitively priced Methanol and potassium hydroxide?
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