***  For details on how to be removed from this list visit the  ***
***          CCP4 home page http://www.ccp4.ac.uk         ***



> As IT said before, a reasonable distance cutoff seems
> feasible. Perhaps 95% of all cases could be distinctly distinguished.

I claim no credit for that idea!  Refmac already uses a distance
threshold to recognise chain breaks.

> 
> The TER record might seem as a means to indicate gaps in the file,
> but that leads to another problem: some check programs 
> (haven't deposited
> lately, maybe PDB can comment) complain if OXT is missing at the
> terminal record. However, putting an OXT on a chain that
> continues and requires a N+1, is wrong. This decision requires a 
> cross-check against sequence. Still, it is doable.

This shouldn't be a problem because you would never deposit with the
intra-chain TER records present, they would all be removed prior to
checking/deposition.  They are only needed in the early stages of
refinement (e.g. just after you've done a rigid-body refinement of
individual domains), when using a distance threshold alone may give an
incorrect indication of chain breakage.  I would trust and hope that
structures are never deposited in such a state!  To be on the safe side
in that situation you would probably want to flag _all_ chains breaks
with TER records, regardless of distance.

For a fully refined structure, a distance check (say 2 Ang.? - I've no
idea what value Refmac uses) should be completely reliable in all cases
because it's not likely that you would be depositing with any bonded
C(i)-N(i+1) distances > 2 Ang., or any non-bonded ones < 2 Ang.!

The biggest (and sadly I suspect insuperable!) problem is to get authors
of model building & refinement programs to implement this usage of TER
records (and of course to abandon usage of the residue number as an
indicator of residue connectivity)!

-- Ian

Disclaimer

This communication is confidential and may contain privileged information 
intended solely for the named addressee(s). It may not be used or disclosed 
except for the purpose for which it has been sent. If you are not the intended 
recipient you must not review, use, disclose, copy, distribute or take any 
action in reliance upon it. If you have received this communication in error, 
please notify Astex Therapeutics Ltd by emailing [EMAIL PROTECTED] and destroy 
all copies of the message and any attached documents. 



Astex Therapeutics Ltd monitors, controls and protects all its messaging 
traffic in compliance with its corporate email policy. The Company accepts no 
liability or responsibility for any onward transmission or use of emails and 
attachments having left the Astex Therapeutics domain.  Unless expressly 
stated, opinions in this message are those of the individual sender and not of 
Astex Therapeutics Ltd. The recipient should check this email and any 
attachments for the presence of computer viruses. Astex Therapeutics Ltd 
accepts no liability for damage caused by any virus transmitted by this email. 
E-mail is susceptible to data corruption, interception, unauthorized amendment, 
and tampering, Astex Therapeutics Ltd only send and receive e-mails on the 
basis that the Company is not liable for any such alteration or any 
consequences thereof.



Reply via email to