Do you have crystals? 

Do they diffract? If so, to what resolution?

What resolution do you require to answer your biological question?

F
On Jun 12, 2012, at 7:46 PM, LISA <[email protected]> wrote:

> Hi all,
>  
> My work is to solve huge complex containing 4 different proteins and total 
> molecular weight is about 300 KD. I can purify the complex by co-expression 
> them in E.coli.  This complex contains 8 protein A, 2 protein B and 1 protein 
> C and D. protein B and protein C  have homology structures deposited in PDB 
> database. No homology structure available for protein A and D, which 
> contribute 60% of the whole molecular weight for the complex. 
>  
>       Now I am trying to find a way to solve the phase of this complex. I am 
> thinking of use sad or mad with se-Met.   There total 111 Met residues in 
> this complex. Is it possible to solve this complex by se-Met? Does someone 
> have experience to solve huge complex structure with se-met? It is also very 
> welcome for all the suggestion. Thank you.
>  
> All the best,
>  
> Lisa

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