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Hello Dhana,

use a buffer at least, and some salt - if I remember correctly, gel
filtration resins require 150mM salt concentration for proper
separation (might have been 50mM). Even 150mM may be too little to
keep your protein soluble.

Best,
Tim

On 11/20/2013 09:56 PM, Dhanasekaran Varudharasu wrote:
> Dear Crystallographers,
> 
> I dialysed a 30 kDa protein (Recombinant protein which was eluted
> by 20 mM Tris, 500 mM NaCl, 120 mM imidazole) against water for
> overnight. But it gets precipitated after 12 hours. Can anybody
> give some suggestion to avoid precipitation. Thanks Dhana
> 

- -- 
Dr Tim Gruene
Institut fuer anorganische Chemie
Tammannstr. 4
D-37077 Goettingen

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