It looks like a Hepes?
Padayatti

On Mon, Feb 3, 2014 at 8:37 AM, Annemarie Weber <
[email protected]> wrote:

> Dear all,
> I am refining a 1.4 A resolution structure and found some well-defined but
> unfortunately unexplained density. The protein was purified in HEPES buffer
> with PMSF and protease inhibitor cocktail tablets (Roche) added. It was
> cocrystallized with AMPPNP in PEG2000MME and Tris. I modelled a molecule
> into the density, which fits quite well but I do not know what it is and
> how it got there. Attached are two pictures with the difference density and
> the molecule I modelled in there.
> Has anybody seen something like this before? Maybe some degradation
> product of the buffer/PMSF?
> Any suggestions will be highly welcome.
> Thanks a lot
> Annemarie
>



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