I am late to this discussion and have little to add, but this called me to
comment:

"I did a bit of research. Some authors talk about "intercalation", which
happens below freezing. Intercalation is when the anode becomes plated with
lithium ions instead of the ions being absorbed into the anode."

I don't know the authors referred to, but this is an incorrect definition
of intercalation. Intercalation is the nestling of Li ions between sheets
of graphene in the anode. It happens are all temperatures, not only below
freezing.
[Here is a hoard of images describing intercalation:  <goog_1326516460>
http://tinyurl.com/y46elflk]

Intercalation has nothing to do with Li plating onto the anode.
Intercalation of the ions is what makes Li ion cells so much better than
PbSO4, and why there is little decrease in the state of charge if a cell
sits for a long time. The ions sort of drop into little pockets of the
hexagonal structure of carbon in graphene. It is a stable condition. I base
this on the Waterloo lecture by Dr. Jeff Dahn,and other reference material.
I am old enough to forget stuff, but I am pretty certain of this.

The decrease in cell function due to plating is purely mechanical. The
anode needs to be porous enough that ions pass from the electrolyte easily.
he plating of the Li on the SEI (solid electrolyte interphase) of the anode
simply blocks the passage of ions and reduces their ability to penetrate
the anode. It clogs the screen so to speak. This is not intercalation it is
simple plating.

Clotting up the SEI of the anode nd degredation of the electrolyte are
significant causes of cell dysfunction. the discharged cathode is highly
reactive and mess with the electrolyte. A lot of improvements in Li ion
cells is additives to make the electrolyte less easily damaged when the
cell is fully charged. Heat is also a factor when the cell is fully
charged. This is a good reason to mostly charge no more than 80% or 90% of
100% SOC. It keeps the positive electrode from becoming fully reactive and
starting to tear up the electrolyte.

Back the subject of cold performance. Part of the problem is simply
increased viscosity of the electrolyte leading to lower mobility of the
ions. I am not sure what is going on with electrolyte formulation, but
lower viscosity was one of the main paths of interest 5 years ago.

A little OT: some electrochemists are averse to talking about anodes and
cathodes preferring to refer to the positive and negative electrodes. This
is because the words anode and cathode apparently change meaning depending
on whether a cell is charging or discharging. Referring to positive and
negative electrodes eliminates confusion.

The purchase and application of the graphene has a major effect on cell
capacity. Definitely non-trivial. You don't just smear some carbon on a
sheet of copper. (You could make a Li ion cell in your garage, but it would
be limited by your ability to make a quality application of the graphene.)
Cell capacity 5 years ago was limited by the ability of the graphene to
make proper orientation in the manufactured electrode, and therefore the
availability of sites for intercalation iwas limited. A cell with
theoretically perfect graphene formation would be many times greater in
capacity.

Mike






On Mon, Sep 9, 2019 at 8:12 PM paul dove via EV <[email protected]> wrote:

> You are confusing electric current with a chemical process.
> Ohms law does not apply in a chemical process.
> Low temperatures slow the chemical reaction and charge transfer
> velocity, which leads to the decrease of ionic conductivity in the
> electrolytes and lithium-ion diffusion within the electrodes. Such decrease
> will result in the reduction of energy and power capability, and sometimes
> even performance failure.
>
>
> Sent from my iPhone
> On Sep 9, 2019, at 12:38 PM, Peri Hartman via EV <[email protected]>
> wrote:
>
>
> Hi,
>
> Does anyone have a more in-depth explanation why li ion cells perform
> poorly in cold weather ? It's well known that your range goes down when the
> battery is cold. Lots of writers talk about the phenomena and advise you
> about it but fail to give any real explanations. I think this conversation
> may have come up a long while ago but it's hard to search for.
>
> I did a bit of research. Some authors talk about "intercalation", which
> happens below freezing. Intercalation is when the anode becomes plated with
> lithium ions instead of the ions being absorbed into the anode. Obviously,
> that permanently ruins the battery. So, this is irrelevant regarding poor
> range in cold weather.
>
> I did find one article that might be relevant, though.
>
>
> https://cen.acs.org/articles/96/i10/Rechargeable-battery-weathers-extreme-cold-conditions.html
>
> They claim the electrolyte becomes viscous, slowing down the ion movement.
> That's about all they say. But, I'll add my thoughts.
>
> If the electrolyte is viscous, then I suspect the voltage potential drops.
> Since watts-hours (energy) is V * Ah, you have less energy available,
> assuming that the Ah is constant. But, what about internal resistance ? For
> the same driving behavior, you'll need higher amps at a lower voltage.
> Resistance loss is I^2 * R, so that loss should go up significantly. I'm
> getting into a trap here: why doesn't the increased resistance loss heat up
> the battery ? The nominal resistance is extremely low, so maybe even at an
> elevated state there isn't enough heat to affect the electrolyte's
> viscosity. Don't know.
>
> Here's another article that talks about electrolyte. They talk about
> preventing decomposition of electrolyte.
>
> https://spectrum.ieee.org/energywise/green-tech/fuel-cells/lithium-additives
>
> Obviously, the other major factors are cabin heat and defrost.
>
> Peri
>
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