Much less than triclinic..aperiodic!
Norberto

Inviata dal mio Windows Phone
________________________________
Da: Davide Levy<mailto:[email protected]>
Inviato: ‎10/‎05/‎2015 11.13
A: 'Alan Hewat'<mailto:[email protected]>; 'Leonid 
Solovyov'<mailto:[email protected]>
Cc: 'Lista Rietveld'<mailto:[email protected]>
Oggetto: RE: On the “crystallographic good practices”

I am glad not to be the only one who think that all crystal are triclinic :) .
Are you interested  for a  Rietveld Method group on Facebook ?
Davide

From: [email protected] [mailto:[email protected]] On Behalf Of Alan Hewat
Sent: 10 May, 2015 11:33 AM
To: Leonid Solovyov
Cc: Lista Rietveld
Subject: Re: On the “crystallographic good practices”

Dear Leonid.

You have a point, but they also have other evidence for lower symmetry. 
(Personally I have for long believed, secretly, that all structures were at 
best triclinic, and that everything else was just an average :-) I know you 
like to be provocative, but let's not start a little war over this. Normally 
the referees and journals, together with the authors, are responsible for what 
they publish.

Best wishes, Alan.

On 9 May 2015 at 19:02, Leonid Solovyov 
<[email protected]<mailto:[email protected]>> wrote:
Regarding the query of Leopoldo Suescun:
”Shouldn´t the IUCr take action and try to influence the journals that
frequently publish x-ray data (as a complementary characterization
technique but that determines the validity of other results) to have
well-trained crystallographers review any article that contains x-ray
diffraction data?”

Unfortunately, the issue of crystallographic review is problematic even in the 
IUCr journals, especially for powder data. A fresh instance from Acta B:
http://dx.doi.org/10.1107/S205252061500342X
where the crystal structures of alpha-Fe2O3 and alpha-Cr2O3 are “re-refined” to 
be monoclinic. The monoclinic symmetry is “substantiated” by the observation of 
a “complex” peak broadening that, in fact, is well described by the anisotropic 
strain model available in all popular Rietveld programs.
With such structure validation, all crystal structures may be re-refined, 
potentially, to lower symmetry, as the anisotropic strain broadening is a 
common powder pattern feature.
If this practice is accepted in an IUCr journal, what can we expect from 
non-crystallographic literature?

 *******************************************************
Leonid A. Solovyov
Institute of Chemistry and Chemical Technology
660036, Akademgorodok 50/24, Krasnoyarsk, Russia
http://sites.google.com/site/solovyovleonid
*******************************************************

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--
______________________________________________
   Dr Alan Hewat, NeutronOptics, Grenoble, FRANCE
<[email protected]<mailto:[email protected]>> 
+33.476.98.41.68
        http://www.NeutronOptics.com/hewat
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