I sometimes also get that 'salt' looking thing that Pieter is talking 
about. Mine falls out at the end of the acid stage if I let it sit for a 
few days.
mark

 - I can't imagine anything that would separate the 
> NaOH unless you didn't mix it thoroughly in the first place. Acid 
> would separate it from the glycerine by-product cocktail, but it 
> would need more acid to do that than the amount of sulphuric 
acid 
> specified, which should have been more than neutralised by 
the 
> methoxide anyway. 




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