Hello Jim, when using the acid esterification, you will have methyl esters, unreacted oil, sulphate ions, oxonium ions and - water. Proceeding to the base step you will create more methyl esters, potassium or sodium soaps, maybe a little unreacted oil or partially reacted oil, potassium or sodium sulphates and - even more water. This method works fine if the water content can be kept on a reasonable level. Please note that the higher the initial FFA level, the more water will be produced. With best regards Jan Jan Warnqvist AGERATEC AB
[EMAIL PROTECTED] + 46 554 201 89 +46 70 499 38 45 ----- Original Message ----- From: "JJJN" <[EMAIL PROTECTED]> To: "BIO" <Biofuel@sustainablelists.org> Sent: Thursday, January 05, 2006 3:01 AM Subject: [Biofuel] Acid - Base questions > I have decided to try the acid/base method in small test batches as I > have some High FFA (4ml) oil I would like to process. Since September I > have gone to great lengths to get repeatability and accuracy in all my > work with Biodiesel. I have read and re-read JtF and I know that I will > no doubt read it several more times if I get stumped. I would like to > start with fully understanding the process first. > Before I start: > Can you use KOH with the Acid Base method? It might be obvious, but I > did not see it in the recipe as a substitution. > > When the acid gets done with Estrification properly then the mix that is > left is basically an oil (triglycerides) , Methanol, and Sulfur ions ? > Or did I miss something? > > When the Methoxil is added the Sulfur gets combined with the Sodium > ions, (right?) how does this affect the reaction? > > Any good experienced information would be helpful, > > Jim > > _______________________________________________ > Biofuel mailing list > Biofuel@sustainablelists.org > http://sustainablelists.org/mailman/listinfo/biofuel_sustainablelists.org > > Biofuel at Journey to Forever: > http://journeytoforever.org/biofuel.html > > Search the combined Biofuel and Biofuels-biz list archives (50,000 messages): > http://www.mail-archive.com/biofuel@sustainablelists.org/ > > _______________________________________________ Biofuel mailing list Biofuel@sustainablelists.org http://sustainablelists.org/mailman/listinfo/biofuel_sustainablelists.org Biofuel at Journey to Forever: http://journeytoforever.org/biofuel.html Search the combined Biofuel and Biofuels-biz list archives (50,000 messages): http://www.mail-archive.com/biofuel@sustainablelists.org/