Hello Jim,
when using the acid esterification, you will have methyl esters, unreacted
oil, sulphate ions, oxonium ions and - water.
Proceeding to the base step you will create more methyl esters, potassium or
sodium soaps, maybe a little unreacted oil or partially reacted oil,
potassium or sodium sulphates and - even more water.
This method works fine if the water content can be kept on a reasonable
level. Please note that the higher the initial FFA level, the more water
will be produced.
With best regards
Jan
Jan Warnqvist
AGERATEC AB

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----- Original Message ----- 
From: "JJJN" <[EMAIL PROTECTED]>
To: "BIO" <Biofuel@sustainablelists.org>
Sent: Thursday, January 05, 2006 3:01 AM
Subject: [Biofuel] Acid - Base questions


> I have decided to try the acid/base method in small test batches as I
> have some High FFA (4ml) oil I would like to process.  Since September I
> have gone to great lengths to get repeatability and accuracy in all my
> work with Biodiesel. I have read and re-read JtF and I know that I will
> no doubt read it several more times if I get stumped.  I would like to
> start with fully understanding the process first.
> Before I start:
> Can you use KOH with the Acid Base method?  It might be obvious, but I
> did not see it in the recipe as a substitution.
>
> When the acid gets done with Estrification properly then the mix that is
> left is basically an oil (triglycerides) , Methanol,  and Sulfur ions ?
> Or did I miss something?
>
> When the Methoxil is added the Sulfur gets combined with the Sodium
> ions, (right?) how does this affect the reaction?
>
> Any good experienced information would be helpful,
>
> Jim
>
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