Hi!

I came accross this statistics issue and am hoping to get some
suggestions from here. As part of our experiment design we have a need
to statistically quantify the number of bacteria in a bag of medium.
The goal is to be able to say that the bag is bacteria-free after
evaluating some sampels taken from the bag.
The size of the total medium is 50 ml for the bag and the volume of
sample taken for evaluation is 0.5 ml.

My first thought is to divide the bag into 100 units of 0.5 ml. For
each sample, it's either bacteria-positive or bacteria-negative. From
there, if I use a bionomial approach to test bwteen 1% and 40%
bacteria+ by approximating wth normal distribution, I come up with n=5
(sample size) for 0.05 level of significance and 95% power. The issue
is that since it's small sample size with small porpotion (that is
np<5), I don't know if using normal distribution approximation is
justified. For pratical reason, a large sample size >10 is usually not
attainable.

Any other thoughts, for example, not to use bionomial approach, or to
set any criteria for quantifying the number of bacteria in a bag
(50ml) by sampling (0.5 ml each) is highly welcome!

Thank you for any advice!
.
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