I really like the update on your page! Yove made quite some progress :)

On Sunday, June 17, 2012 8:53:26 PM UTC+1, Dalibor wrote:
>
> Nice information about making stems are in the Roth's book noticed 
> recently here.. "Vacuum sealing techniques", for those interested in this 
> book, let me know outside, I will post link..
>
> I have already got a small test mold made from graphite, 13-pin.. My 
> original intention was to arrange some kind of furnace in microwave oven 
> and melt the glass directly in the mold with dumet wires inside.. But no 
> luck yet, I am able to heat a piece of the carbide to 1000C, but the power 
> is to small to heat all the mold with glass. Another thing is, that at this 
> temperature, the graphite reacts with oxygen producing CO2 and degrades.. I 
> think 10 cycles is maximum for one mold. The furnace with controlled 
> atmosphere (nitrogen, argon, CO2 ..) would be the best.. I am going to ask 
> my friend to test that process in their lab, he has a special tubular 
> furnace able to go above 2000C ;-)
>
> I am preparing some short blogpost about my fail ;-) I will publish it 
> tonight. Except that, I had also some small success, sealed argon tubes.. 
> that post is already done:
>
> http://dalibor.farny.cz
>
> Dalibor
>
> 2012/6/17 Dalibor Farný <dali...@farny.cz>
>
>> Hi John,
>>
>> are You sure that only gravity is enough for the glass to flow to the 
>> mold? At what temperatures? I tried 800C and no luck..
>>
>> Dalibor
>>
>>
>> 2012/6/17 John Rehwinkel <jreh...@mac.com>
>>
>>> > How exactly would you proceed making - say - 13 pin tube bases? You 
>>> need a lot of temperature for that and precisely formed tools. So far this 
>>> is nothing I can see myself doing in the near future. I know a person who 
>>> makes his own (borosilicate glass) sockets, I might be able to adopt the 
>>> principle some day.
>>>
>>> The tool part isn't too tough, just carve it out of graphite with pin 
>>> recesses.  CNC machining would be the way I'd go, but back in the day it
>>> was done by reading scales on handwheels, and obviously it could still 
>>> be done that way.  Once you have your graphite mold/pin holder,
>>> get some nice 3-part pins and lead glass tubing of an appropriate 
>>> diameter.  Lead glass is the way to go here - it liquifies enough to
>>> gravity flow into molds like this.  Slice off rings that have sufficient 
>>> glass to make your bases, drop pins into your mold, put the glass ring
>>> around them, and melt the whole shebang.  For extra niceness, you can 
>>> have an upper mold half that forms little mounds of glass over
>>> the pins themselves and flattens the rest of the base into a disc.  Let 
>>> it cool, and violà!  The first one will be a real bear, as you have to
>>> make the molds determine the amount of glass, temperature to use, etc. 
>>>  But once you have the molds made and the procedure down,
>>> you can knock out additional bases fairly easily.
>>>
>>> - John
>>>
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>>
>>
>> -- 
>> Dalibor Farny
>> http://dalibor.farny.cz
>>
>>
>>
>
>
> -- 
> Dalibor Farny
> http://dalibor.farny.cz
>
>
>

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