On Thursday, 12 February 2015 14:20:39 UTC, johnk wrote:
>
>  
> Maybe I am missing something when it comes to the way this works, but, 
> when it is not a vacuum as is required for a valve/tube then what about the 
> idea of pump a bit, add some of the eventual gas, pump again etc. The 
> original impurities would distribute 'evenly' through the added gas and 
> when it was pumped out a percentage of that older pollutant would be 
> removed again. Thus it seems to me that a quite 'feeble' pump can do the 
> job when the eventual fill is a gas [even if at a lowish pressure]
>

There are many issues involved in making tubes, and getting the right 
pressure and gas mix is just a small part. The glass, and all the other 
mechanical components, contain impurities that have to be removed during 
manufacture else they will taint the behaviour and life-span of the 
finished tube.

Impurities are found in all components, - moisture and other organic and 
non-organic contaminants will even embed in the glass walls and survive the 
initial chemical cleaning phases - these contaminants have to be baked out 
under a decent vacuum, typically around 1 micron (10-3 Torr) which is about 
1/750,000 of an atmosphere. Whilst this sounds like a high vacuum, its 
actually pretty easy to obtain with straight-forward kit. A TM pump is 
distinctly over-kill (several orders of magnitude better), but, hey, if you 
have one, then flaunt it baby! (slight paraphrase there from Zero Mostel!).

Even small levels of contaminants will cause quality problems.To avoid 
this, the tube is baked (various techniques exist for this) to release the 
contaminants whilst being pumped to about 10-3 Torr - the pumps remove 
almost all the cr*p. Then the pumps are sealed off and an amount of the 
highly pure nobel gas being used is let back in - in the case of nixies, 
this will be about 99% neon and 1% argon at a pressure of about 30 Torr - 
about 1/25th of atmospheric pressure - and the tubulation is sealed.

The above is a very simple explanation - it does not explain about 
induction heating or "Bombardment" or how mercury is introduced etc. but 
the principles are the same.

Nick

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