Hello everyone, I am using GSAS for refinement of a zeolite + template assembly. During the 1st few cycles of the refinement, the calculated peaks I am getting are very small although apparently in the right positions. The difference between the observed and calculated intensities is almost an order of magnitude. Refining the profile type and coefficients is not making much of a difference. Since I have no clue as to why there is such a difference, I wanted to simply scale up the calculated values to see how they match up with the observed peaks. I tried using powplot and liveplot, but could not figure out a way to do it. Is such thing possible with GSAS?
Thanks for your attention. Regards, Ramdas Pophale. ps: I am using the template as part of the phase with bond constraints. Is it reasonable to refine the template along with the zeolite in the early stages?
