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The Cookbook is in the signal...
Written by Robert Greenyer on 22 February 2016.
Prepare thoroughly (Ni + LiAlH4 + Li)
Bake Ni
Reduce Ni
Hydrogenate Ni
Mix: Ni + LiAlH4 + Li
Bake and vac reactor, add Nickel, vac warm, add H2, Vac
Heat to above Mössbauer determined Ni Debye (say 135C), pressure regulated
to approx 1bar abs.
Hold, pressure regulated to approx 1bar abs.
Heat slowly to as close to Ni Curie as comfortable (Say 340C), pressure
regulated to approx 1bar abs.
Hold, pressure regulated to approx 1bar abs.
Slowly lower temp to above highest known Ni Debye (Say 220C), pressure
regulated to approx 1bar abs.
Hold, pressure regulated to approx 1bar abs.
Go as fast as possible through Ni Curie
Hold, pressure regulated to approx 0.5bar abs.
Cycle through 500C internal, pressure regulated to approx 0.5bar abs.
Hold, pressure regulated to approx 0.5bar abs.
Raise internal temperature to over 1200, pressure regulated to approx
0.5bar abs.
Drop to around 1000C and hold, pressure regulated to approx 0.5bar abs.
Raise internal temperature to near boiling point of Lithium
Some of the above steps may in time be redundant.
1h Thermal > x/β- emissions > Pb > IR/THz > 5h (SSM)

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2016-02-23 21:37 GMT-03:00 Finlay MacNab <finlaymac...@hotmail.com>:

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