Right: I found out my filtering also removed a foamy white stuff, leaving
the BD clear.

----- Original Message -----
From: "Paul Gobert" <[EMAIL PROTECTED]>
To: <biofuel@yahoogroups.com>
Sent: Saturday, April 27, 2002 7:46 PM
Subject: Re: [biofuel] murky


>
> ----- Original Message -----
> From: "Christian" <[EMAIL PROTECTED]>
> [snip]
>
> >Anyway, I don«t
> > quite understand how filtering removes cloudiness that comes from liquid
> > particles (either water or glycerides).
>
> Christian, the material that my filtration removes is more of a white
soapy
> mature than water or glycerides. It looks much the same colour as clean
> white tallow but it is more uniform in consistency and does not set at
room
> temp.
>
> >My reaction times were, I admit it,
> > perhaps too short. I mixed four independent 1 liter batches, and they
were
> > each left to react for about 30 to 40 minutes. The reaction "seemed"
> > complete after 10 minutes or so, and I thought 30-40 min would do.
>
> In light of what Todd and others have reported I have extended my mixing
> times.
> This may improve the clarity of the BD but I think my use of conc aqueous
> NaOH is a contributing factor.
> Strangely enough results from a test using varying levels of NaOH, with a
> fixed level of methanol on the same feedstock, gave clearer  unwashed BD
for
> higher levels of NaOH than optimum (titration) or low levels. Viscosity
and
> SG were also lower for high levels of NaOH. These tests bear repeating as
> the mixing was of short duration. I suspect that optimum mixing would
level
> out the differences.
>
> Regards,
> Paul Gobert.
>
>
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