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The data is collected to 1.7 A. Is there a way to contrain the As-Ligand bond lengths in another way and use all other As parameters? I know what the distance should be from EXAFS. Thanks for your input
Debbie

Quoting Philippe DUMAS <[EMAIL PROTECTED]>:

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Hello

At which resolution did you collect your data ? If it was not terribly high
(say, not better than 1 Angstrom), I do not think it would be so much a
problem of using As parameters. At most, occupancies and B-factors will be
slightly wrong, but I doubt this would prevent you from refining your
structure.
Probably more problematic (and deterious to the quality of your structure)
is the correct recognition of the bound ligands.

Philippe Dumas
IBMC-CNRS, UPR9002
15, rue René Descartes 67084 Strasbourg cedex
tel: +33 (0)3 88 41 70 02
[EMAIL PROTECTED]



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I have an As(III) ion in my structure.  I am using refmac for
refinement, As(III) is not in the atomsf library.  Does anyone know how
to modify the existing file for As(0) file and add it to the library?
Thanks
Debbie
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