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Dear Paul,

sometimes NOT removing all sugars might even be a good thing. 
See for example, the case of quercetin 2,3 dioxygenase (quercetinase) from
A.japonicus where sugar chains are involved in the formation of a homodimer.
We never managed to remove all sugars and the protein crystallized very well.
(Crystals diffracted too, btw)

Roberto



Quoting Paul McEwan <[EMAIL PROTECTED]>:

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> 
> 
> I'm currently working with a glycoprotein and am having great difficulty
> deglycosylating it for crystallisation. I can completely remove the sugars
> very easily when the protein is denatured (not much good when you're wanting
> to crystalise it), but seems completely resistant to treatment with endo H or
> pngase F when done under native conditions. Any hints on getting this to work
> would be greatly appreciated. 
> 
> ##################################
> Dr Paul A. McEwan
> Protein Crystallography Group
> Centre for Biomolecular Science
> Clifton Boulevard
> University of Nottingham
> Nottingham
> NG7 2RD
> Tel: 0115 8468009
> http://www.nottingham.ac.uk/~pazxtal
> ##################################
> 
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-- 
Dr. Roberto Steiner
Randall Division of Cell and Molecular Biophysics
New Hunt's House
King's College London
Guy's Campus
London, SE1 1UL
Phone +44 (0)20-7848-8216
Fax   +44 (0)20-7848-6435
e-mail [EMAIL PROTECTED]
 

 

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